Frédéric Vogel

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Particle Size Effects in Ru/CNF Catalysts during Supercritical Water Gasification of Glycerol

Oliver Kröcher, Frédéric Vogel, David Baudouin, Ayush Agarwal

Ru/CNF catalysts of different Ru nanoparticle (NP) sizes (0.9-2.7 nm) were assessed for their performance in continuous supercritical water gasification (SCWG) of glycerol. A structure sensitivity of Ru was demonstrated, with high initial turnover frequenc ...

2022

Investigating active phase loss from supported ruthenium catalysts during supercritical water gasification

Oliver Kröcher, Frédéric Vogel, Mohamed Tarik, David Baudouin

Active phase loss mechanisms from Ru/AC catalysts were studied in continuous supercritical water gasification (SCWG) for the first time by analysing the Ru content in process water with low limit-of-detection time-resolved ICP-MS. Ru loss was investigated ...

2021

Mechanochemistry-assisted hydrolysis of softwood over stable sulfonated carbon catalysts in a semi-batch process

Frédéric Vogel, Oliver Kröcher, David Ferdinand Scholz

The hydrolysis of lignocellulose is the first step in saccharide based bio-refining. The recovery of homogeneous acid catalysts imposes great challenges to the feasibility of conventional hydrolysis processes. Herein, we report a strategy to overcome these ...

2019

Deactivation and Regeneration of Sulfonated Carbon Catalysts in Hydrothermal Reaction Environments

Oliver Kröcher, Frédéric Vogel

The deactivation pathways of sulfonated carbon catalysts prepared from different carbons were studied during the aqueous‐phase hydrolysis of cellobiose under continuous‐flow conditions. The sulfonation of carbon materials with a low degree of graphitizatio ...

2018

Fate and reuse of nitrogen-containing organics from the hydrothermal conversion of algal biomass

Christian Ludwig, Frédéric Vogel, Eya Nicodeme, Gaël Peng, Mariluz Bagnoud

2018

Catalytic Supercritical Water Gasification: Continuous Methanization of Chlorella vulgaris

Christian Ludwig, Frédéric Vogel, Gaël Peng, Dominik Refardt

Continuous catalytic supercritical water gasification (CSCWG; 400 degrees C, 28 MPa) of microalgal biomass (Chlorella vulgaris) was carried out at the microalgae production site of ZHAW in Wadenswil (Switzerland) nonstop over a period of 100 h. Microalgae ...

American Chemical Society2017

Catalytic supercritical water gasification: Interaction of sulfur with ZnO and the ruthenium catalyst

Christian Ludwig, Frédéric Vogel, Gaël Peng

Elsevier2017

Ruthenium Dispersion: A Key Parameter for the Stability of Supported Ruthenium Catalysts during Catalytic Supercritical Water Gasification

Christian Ludwig, Frédéric Vogel, Gaël Peng

The catalytic supercritical water gasification of isopropanol (450 degrees C, 30 MPa) over Ru catalysts supported on carbon and metal oxides was performed in a fixed-bed plug flow reactor. The Ru loading was between 1.2 and 2%. The catalyst stability over ...

Wiley-VCH Verlag2016

First developments towards closing the nutrient cycle in a biofuel production process

Christian Ludwig, Frédéric Vogel, Gaël Peng, Mariluz Bagnoud

Hydrothermal liquefaction (HTL) of microalgae is a promising technology offering production of biofuels in a sustainable way. Thanks to the supercritical conditions applied, the recycling of water and nutrients including carbon capture becomes feasible(1-2 ...

Elsevier Science Bv2015

Effect of carbon surface functional groups on the synthesis of Ru/C catalysts for supercritical water gasification

Christian Ludwig, Frédéric Vogel, Gaël Peng

A carbon support was treated with HNO3 to create surface functional groups (e.g. -COOH, -OH), which were then characterized by TGA, TPD, CNS elemental analysis, and Boehm titration. HNO3 modified the carbon surface properties by adding a high amount of car ...

Royal Soc Chemistry2015

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Ruthenium Dispersion: A Key Parameter for the Stability of Supported Ruthenium Catalysts during Catalytic Supercritical Water Gasification

Christian Ludwig, Frédéric Vogel, Gaël Peng

Wiley-VCH Verlag2016

First developments towards closing the nutrient cycle in a biofuel production process

Christian Ludwig, Frédéric Vogel, Gaël Peng, Mariluz Bagnoud

Elsevier Science Bv2015

Catalytic supercritical water gasification: Interaction of sulfur with ZnO and the ruthenium catalyst

Christian Ludwig, Frédéric Vogel, Gaël Peng

Elsevier2017