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A Cp*Rh(III)-catalyzed C-H/C-C bond activation sequence of cyclopropyl hydroxamates has been developed. The three-component process allows trapping of the intermediate rhodacycle with diazomalonates and an alcohol nucleophile to provide access to synthetically valuable alpha-alkoxylated gamma-lactams with trans diastereoselectivity.
Pierre Vogel, Inmaculada Robina, Claudia Bello, Yolanda Vera-Ayoso
Jérôme Waser, Matthew Wodrich, Paola Caramenti, Romain Gaëtan Tessier, Nina Declas
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