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We studied using x-ray photoelectron spectroscopy the deposition of Au, In, Ag and Al overlayers onto clean-cleaved GaTe(001) surfaces at room temperature. The first steps of the Schottky barrier formation on Au and In showed no interface reactions. Free T ...
Segmented flow comprising discrete volumes of a liquid reaction mixture separated by discrete volumes of immiscible fluid is passed through a tubular reactor for residence times sufficient to precipitate a powder product from the reaction mixture. USE-Manu ...
An experimental procedure has been designed in order to trace interactions within the binder responsible for the setting properties (flow decay + strength) of Low Cement Castables (LCC). After mixing, the binders which have been studied are characterized b ...
1-Bromo-3,5-bis(trifluoromethyl)benzene was selectively prepd. by treatment of 1,3-bis(fluoromethyl)benzene with N,N'-dibromo-5,5-dimethylhydantoin in strongly acidic media. A no. of synthetically useful reactions via 3,5-bis(trifluoromethyl)phenylmagnesiu ...
HOBr can be formed in various oxidation processes in engineered and natural systems. The rate of HOBr reduction by H2O2 is decisive to avoid formation of brominated organic compounds and bromate during ozone or hydrogen peroxide-based advanced or naturally ...
N,N-dimethylhydrazones,e.g., CH2:CFCH:NNMe2, prepd. from 2-fluoro-2-alkenals undergo smooth [4 + 2] cycloaddn. reactions with Me acrylate, di-Me acetylenedicarboxylates and quinones. The resulting 3-fluoropyridines, e.g., I, or dihydro and tetrahydro deriv ...
A process for the production of powders by precipitation from a liquid reaction mixture comprises passing along a tubular reactor a segmented reaction flow comprised of discrete volumes of the reaction mixture separated by discrete volumes of a separating ...
Metal Complexes of Biologically Important Ligands, LXX[1].- Synthesis, Stereochemistry and Reactions of Ruthenium(II) and Osmium(II) Complexes with -Amino Carboxylates. The reactions of MHCl(CO)(PPh3)3 with salts of -amino acids give the hydrido-N,O-chelat ...
An account of our most recent studies on the application of high pressure kinetic techniques in mechanistic studies of inorganic reactions is presented. The investigated reactions include substitution, addition, insertion, elimination, electron-transfer, p ...
We investigated the adsorption properties of methanol and ethanol on Si(111)2 x 1 as a function of temperature in the range 80-300 K by means of synchrotron radiation photoemission of core and valence levels. A physisorbed state is characterized at 80 K, w ...
