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A simple and general procedure has been developed to determine the thermal behaviour of a reactor based on heat balance, PID temperature control, and jacket behaviour. Using only temperature heating/cooling ramps followed by isothermal stages, such a proce ...
Chemical incidents are typically caused by loss of control, resulting in runaway reactions or process deviations in different stages of the production. In the case of fed-batch reactors, the problem generally encountered is the accumulation of heat. This i ...
Schweizerische Chemische Gesellschaft2014
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A new system combining a microreactor and a microcalorimetric chip was investigated. The small size of the microreactor channel permits maintaining isothermal conditions necessary for the kinetic characterization of highly exothermic reactions. These condi ...
2004
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The specific problem of non-converted reactant accumulation encountered in fed-batch reactor is a challenging task of process safety. In order to avoid such situation that may lead to a runaway reaction, the reaction kinetics and reactor dynamic must be kn ...
Aidic Servizi Srl2016
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Most processes in the chemical industry involve potentially hazardous steps. It is thus of critical importance to perform risk assessments and to know the thermal behavior of the chemicals at stake. A widely used thermal analysis, differential scanning cal ...
Wiley-Blackwell2015
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For efficient inherently safe design, awareness of all available options at the appropriate decision-making moment is key. Simulations offer both timely availability and large screening possibilities. Therefore computer-aided product design gained in popul ...
Aidic Servizi Srl2016
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Handling and storing chemicals in the industrial world require a conscientious hazards assessment and the implementation of appropriate measures to ensure safety for the workers, the company, the environment and the society. Reliable evaluations and predic ...