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Cyclodepsipeptides incorporating a sugar amino acid, e.g., I, have been synthesized. A three-component reaction of a sugar amino acid (SAA) deriv., an aldehyde, and a dipeptide isonitrile in refluxing methanol afforded the corresponding 5-aminooxazole which, after sapon., underwent a trifluoroacetic acid promoted macrocyclization to furnish the cyclic sugar amino acids. [on SciFinder (R)]
Rolf Gruetter, Hikari Ananda Infinity Yoshihara, Alice Radaelli
Horst Vogel, Horst Pick, Olivia Baud, Sylvain Etter