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New schemes are introduced that allow one to improve the resolution in the indirect dimension of single-scan 'ultrafast' two-dimensional NMR spectra. The methods combine undersampling with band-selective pulses to recover signals that lie outside the detection bandwidth. The efficiency is illustrated for homonuclear total correlation spectroscopy (TOCSY) of quinidine. (C) 2008 Elsevier Inc. All rights reserved.
Majed Chergui, Andre Al Haddad, Lars-Hendrik Mewes, Rebecca Ann Ingle