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Sensitivity in Nuclear Magnetic Resonance (NMR), especially in solid-state NMR, has always been a challenging and important issue and thus a motivation for new developments. The magnetic field B0, the gyromagnetic ratios of the observed nuclei, as well as ...
Nuclear magnetic resonance (NMR) was discovered in the first half of the 20th century. Today, neither analytical chemistry without NMR spectroscopy nor medical diagnostics without magnetic resonance imaging (MRI) could be imagined. A magnetic resonance sig ...
Searching for optimal conditions during one- and multi-dimensional solid-state NMR experiments in high static fields may require spinning the sample at frequencies above 40 kHz. This implies challenging requirements for heteronuclear spin decoupling. We ha ...
We demonstrate that high field (9.4T) dynamic nuclear polarization (DNP) at cryogenic (similar to 100 K) sample temperatures enables the rapid acquisition of natural abundance H-1-H-2 cross-polarization magic angle spinning (CPMAS) solid-state NMR spectra ...
Dynamic nuclear polarisation (DNP) has been used to obtain magic angle spinning (NOT)-N-14 (nitrogen-14 overtone) solid-state NMR spectra from several model amino acids, with both direct and indirect observation of the (NOT)-N-14 signal. The crystalline so ...
Electronic and magnetic properties of quasi-one dimensional ormore widely low-dimensional systems aswell as their related correlated electron phenomena have been at the very frontier of condensed matter physics for quite some time. The reduced dimensionali ...
This thesis describes new methods for the detection of 14N nuclei by solid-state nuclear magnetic resonance. So far, the low natural abundance (0.4 %) 15N isotope has been widely used to study nitrogen-containing samples because of its spin-1/2 nature. The ...
The Fourth European Microwave Conference, held in 1974 in Montreux, Switzerland, was the first one organized professionally with a commercial exhibition, Microwave'74. Joining two basically different events required a careful preparation, with many discuss ...
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A general approach for structural interpretation of local disorder in partially ordered solids is proposed, combining high-resolution two-dimensional (2D) nuclear magnetic resonance (NMR) and first principles calculations. We show that small chemical shift ...
By using the Telospot assay, 27 different extracts of cyanobacteria were evaluated for telomerase inhibition. All extracts showed varying, but significant activity. We selected Microcystis aeruguinosa PCC 7806 to identify the active compound and a bioassay ...