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Advanced characterization of regioselectively substituted methylcellulose model compounds by DNP enhanced solid-state NMR spectroscopy

Related publications (35)

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Environmental and taxonomic controls of carbon and oxygen stable isotope composition in Sphagnum across broad climatic and geographic ranges

Luca Bragazza, Mariusz Lamentowicz, Bjorn Jozef Maria Robroek

Rain-fed peatlands are dominated by peat mosses (Sphagnum sp.), which for their growth depend on nutrients, water and CO2 uptake from the atmosphere. As the isotopic composition of carbon (C-12(,)13) and oxygen (O-16(,)18) of these Sphagnum mosses are affe ...

COPERNICUS GESELLSCHAFT MBH2018

Solid-state NMR at natural isotopic abundance for the determination of conformational polymorphism - the case of designed beta-turn peptides containing di-prolines

Jayasubba Reddy Yarava, Rajesh Sonti

The proton double quantum-carbon single quantum correlation experiment has been applied to designed peptides in the solid state in natural isotopic abundance. Analogous to nOe studies in solution, through-space double-quantum connectivities have been explo ...

Royal Soc Chemistry2017

Environmental drivers of carbon and nitrogen isotopic signatures in peatland vascular plants along an altitude gradient

Alexandre Buttler, Konstantin Svetlozarov Gavazov, Luca Bragazza

Peatlands are important sinks of atmospheric carbon (C) that, in response to climate warming, are undergoing dynamic vegetation succession. Here we examined the hypothesis that the uptake of nutrients by different plant growth forms (PGFs) is one key mecha ...

Springer2016

Disinfection processes such as chlorination, chloramination, and ozonation are a crucial measure to provide safe drinking water because they effectively inactivate pathogenic microorganisms. However, these processes can also lead to the formation of harmfu ...

EPFL2016

A solid-state NMR method to determine domain sizes in multi-component polymer formulations

David Lyndon Emsley, Judith Schlagnitweit

Polymer domain sizes are related to many of the physical properties of polymers. Here we present a solid-state NMR experiment that is capable of measuring domain sizes in multi-component mixtures. The method combines selective excitation of carbon magnetiz ...

Academic Press Inc Elsevier Science2015

Copper isotope evidence for large-scale sulphide fractionation during Earth’s differentiation

James Badro

The differentiation of Earth into a metallic core and silicate mantle left its signature on the chemical and isotopic composition of the bulk silicate Earth (BSE). This is seen in the depletion of siderophile (metal-loving) relative to lithophile (rock-lov ...

2015

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We show how dynamic nuclear polarization (DNP) enhanced solid-state NMR spectroscopy can be used to characterize polymorphs and solvates of organic solids. We applied DNP to three polymorphs and one hydrated form of the asthma drug molecule theophylline. F ...

American Chemical Society2015

Uranium Isotopes Fingerprint Biotic Reduction

Rizlan Bernier-Latmani, Yuheng Wang, Malgorzata Alicja Stylo

Knowledge of paleo-redox conditions in the Earth's history provides a window into events that shaped the evolution of life on our planet. The role of microbial activity in paleo-redox processes remains unexplored due to the inability to discriminate biotic ...

Natl Acad Sciences2015

Assessment of available water is the basis that allows for sustainable management of the water resource. Special need concerns the assessment of groundwater resources, about which, often little is known. The present study aims to explore the water resource ...

2014

Assessing the pathways and rates of organic pollutant transformation in the environment is a major challenge due to co-occurring transport and degradation processes. Measuring changes of stable isotope ratios (e.g. C-13/C-12, H-2/H-1, N-15/N-14) in individ ...

Swiss Chemical Soc2014