Performance and reproducibility of C-13 and N-15 hyperpolarization using a cryogen-free DNP polarizer
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Nuclear magnetic resonance (NMR) is used for a large array of applications, ranging from chemical characterization to oil drilling to medical imaging. In these fields NMR is used as an investigational tool, but new techniques and applications are continuou ...
This work augments the proposal of Schwarzenbach & Flack [J. Appl. Cryst. (1989), 22, 601-605], who have advocated the use of a diffractometer-independent definition of the azimuthal angle ψ to specify the diffractiongeometry of a Bragg reflection. It ...
A solid-state 13C NMR spectrum, obtained with cross-polarization and magic-angle sample spinning, and a high-resoln. 13C NMR spectrum of a 0.07 M CHCl3 soln. indicated the presence of a 1:1 cis-trans ratio of the PdCl2(PMe2Ph)2 isomers in the solid-state. ...
For most of the last forty years, the techniques of Dynamic Nuclear Polarization (DNP) have been confined to particle-physics laboratories building polarized targets, but recently it has been shown that samples similar to a solid target can be transformed ...
