Composition and Element Distribution Mapping of γ′ and γ" Phases of Inconel 718 by High-Resolution Scanning Transmission Electron Microscopy and X-ray Energy-Dispersive Spectrometry
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Upon solidification, most metallic alloys form dendritic structures that grow along directions corresponding to low index crystal axes, e.g., directions in fcc aluminum. However, recent findings[1,2] have shown that an increase in the zinc content in Al-Zn ...
An Al-6.3Li-0.07Sc-0.02Yb (at.%) alloy is subjected to a double-aging treatment to create nanoscale precipitates, which are studied by atom-probe tomography and transmission electron microscopy. After homogenization and quenching, Yb atoms form clusters ex ...
In the quest of materials for the first wall of the future fusion reactor, it has been shown that oxide dispersion strengthened (ODS) ferritic / martensitic (F/M) steels appear to be promising candidates. The inherent good mechanical properties supported b ...
We study in this thesis the structural origin of defect insensitive light emission in indium containing group-III nitride ternary alloys grown on sapphire, which are the active materials for the commercially available high brightness blue diodes. These str ...
Transmission electron microscopy was performed to investigate the microstructure and precipitates in the annealed Co38Ni33Al29 ferromagnetic shape memory alloy. Apart from the dendritic secondary phase in the austenite matrix, micron-sized (up to 100 μm) f ...
Precipitation hardening remains an important and efficient way to improve the mechanical resistance of aluminium alloys. In the case of the Al-Mg-Si system (6XXX series), a complex precipitation sequence occurs, which is greatly affected by the presence of ...
The electron microscopy community makes a wide use of Energy Dispersive X-ray Spectrometry (EDS) for elemental mapping in STEM. This technique was however long reckoned slow, dozens of minutes if not an hour, to collect enough information for one map. Rece ...
A comprehensive modelling approach has been developed for the simulation of microstructure formation during solidification and heat treatment in Ni-base superalloys. The microsegregation taking place during solidification is simulated using the pseudo-fron ...
In imaging and focusing applications, spherical aberration induces axial broadening of the point spread function (PSF). A transparent medium between lens and object of interest induces spherical aberration. We propose a method that first obtains both the p ...
A surface-supported open metal−organic nanomesh featuring a 24 nm2 cavity size and extending to μm domains was fabricated by Co-directed assembly of para-hexaphenyl-dicarbonitrile linker molecules in two dimensions. The metallosupramolecular lattice is the ...