Synthesis and structural elucidation of a "free" phosphinoamide anion
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cf. CA 55, 23400c. The Cu salt decompn. of diazo compds. in the presence of Ph3P opens up a new path to the synthesis of phosphorus-ylides. Ph3P (10 millimoles) and 10 millimoles 0.6M CH2N2 in Et2O treated 15 min. with 1 millimole anhyd. CuCl in 70 ml. tet ...
The reaction of the cluster complexes [Pt-3(mu -CO)(3)(PR3)(3)] (PR3 = PPh3 1, PPh(2)Bz 2, PCy3 3 and P(i)pr(3) 4) with dialkyl acetylenedicarboxylate, R'O2CC drop CCO2R' (R= CH3 or Bu-t) have been examined under various conditions. At low temperature the ...
