Oxidation of carboxylic acids at boron-doped diamond electrodes for wastewater treatment
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Six different fluoroarenes were submitted to the same transformations. Direct deprotonation with alkyllithium or lithium dialkylamide as reagents and subsequent carboxylation afforded acids. These included 2,6-difluorobenzoic acid, 3,6-difluoro-2-iodobenzo ...
The electrochem. oxidn. of phenol at synthetic boron-doped diamond thin film electrode (BDD) was studied in acid media by cyclic voltammetry, chronoamperometry, and bulk electrolysis. In the potential region of water stability (E
The electrochem. oxidn. of 3-methylpyridine (3-MP) at synthetic boron-doped diamond (BDD) thin film electrode was studied in acid media by cyclic voltammetry and bulk electrolysis. The results showed that in the potential region of water stability there ca ...
Synthetic boron-doped diamond (BDD) thin film electrodes were tested for the electrogeneration of silver(II). In nitric acid, the kinetics of the silver(I)/silver(II) couple were studied by cyclic voltammetry. The results demonstrate that silver(II) can be ...
Novel three-component domino processes to polyheterocycles are developed. Reaction of an allylamine, an aldehyde and an alpha -isocyanoacetamide in methanol at room temp. provides an efficient access to an oxa-bridged tricycle as a single diastereoisomer. ...
B-doped diamond films were deposited by large-area hot filament chem. vapor deposition (HFCVD) on Si and different industrial electrode materials, such as Ti, Zr, Nb, Ta, W, and graphite, with areas up to 50 * 60 cm2. B-doping levels ranging from 50 to sev ...
The electrochem. oxidn. of benzoic acid (BA) was studied on boron-doped diamond electrodes on acid medium by cyclic voltammetry and bulk electrolysis. In the potential region where the supporting electrolyte is stable, reactions occur, resulting in the los ...
A deprotonation study was performed using 2,3,5-trichloropyridine, 3,5-dichloro-2-fluoropyridine, and 5-chloro-2,3-difluoropyridine as the substrates. Upon reaction with lithium diisopropylamide (LDA), deprotonation occurred exclusively at the 4-position. ...
Boron doped diamond films have been deposited by large area hot-filament CVD (HFCVD) on silicon, silicon carbide, and different industrial electrode materials, like niobium, tantalum, titanium, tungsten, zirconium, and graphite on areas up to 40 cm * 60 cm ...
Cyclic voltammetry for the ferri-ferrocyanide redox couple was used to study the Ti/SnO2-Sb2O5 electrode prepd. by spray-pyrolysis under different conditions. Increasing the prepn. temp. and the duration of coating deposition results in a decrease of ip an ...
