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After assessing the current status concerning the interpretation of Si 2p core-level shifts in Si-O systems, we model the atomic structure of the Si(001)-SiO2 interface using recent photoemission data obtained with synchrotron radiation. Our model structur ...
The reproducible synthesis of the unusual ionic aluminum compd. [Tl3F2Al(OR)3]+[Al(OR)4]- (1) is reported. In the reaction of Li[Al(OR)4] [R = C(H)(CF3)2] with TlF the initially desired Tl[Al(OR)4] only formed with an exact 1:1 stoichiometry, while an exce ...
Ferritic/martensitic steels considered as first-wall candidate materials for fusion reactors experience significant radiation hardening at temperatures below similar to400 degreesC. Experimental evidence suggests that the observed defects are large interst ...
The reaction of the cluster complexes [Pt-3(mu -CO)(3)(PR3)(3)] (PR3 = PPh3 1, PPh(2)Bz 2, PCy3 3 and P(i)pr(3) 4) with dialkyl acetylenedicarboxylate, R'O2CC drop CCO2R' (R= CH3 or Bu-t) have been examined under various conditions. At low temperature the ...
Using a first-principles approach, we assign N 1s core-level shifts at ammonium exposed Si(001)2x1 surfaces to definite bonding configurations of N atoms. Model structures are obtained by fully relaxing the atomic positions of N atoms in different bonding ...
The dynamic range, sensitivity and dark decay of holographic recording in LiNbO3 crystals doped with 0.2 atomic% Mn with different oxidation states have been measured. The sensitivity is 0.5 cm/J and found to be independent of the oxidation states, while t ...
A transmission electron microscopy of pyramidal inversion domains induced by Mg doping in MOVPE and bulk GaN is presented. Based on high resolution observations and EDX analysis, two atomic models are proposed for the Mg-rich (0001) inversion domain bounda ...
A release technique that enables to lift microfabricated structures mechanically off the surface without using wet chemistry is presented. A self-assembled monolayer of dodecyltrichlorosilane forms a very uniform 1.5-nm-thick anti-adhesion coating on the s ...
A new cubic Ta-bronze (1) KTa1+z+(5-delta)O3 [z similar or equal to 0.107 (3)] was obtained on a cathode by molten salt electrolysis of the system K2TaOF5-K3TaO2F4-(KF + NaF + LiF)(cutectic). Black, metallic cubic crystals of (1) are formed together with t ...
We report the in-plane (rho (ab)) and out-of-plane (rho (c)) resistivities in the 4-800 K range on single crystals of Tl2Ba2CaCu2O8 high-T-c cuprate with T-c = 111 K (rho (c)/rho (ab) approximate to 1000). rho (ab)(T) exhibits "usual" linear behavior and r ...