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The modulation of spin echoes by homonuclear scalar couplings render the determination of transverse relaxation rates of individual spins difficult, in particular for molecules that are isotopically enriched in 13C or 15N, and for all molecules with scalar-coupled protons. To avoid echo modulations, most studies using refocusing pulses have so far been restricted to isolated 1H, 13C, or 15N spins. We report measurements of apparent 1H transverse relaxation rates of backbone and side-chain protons in Cyclosporin A (CsA) determined by quenching the echo modulations that arise from homonuclear scalar couplings between protons.
Jian Wang, Matthias Finger, Lesya Shchutska, Qian Wang, Matthias Wolf, Varun Sharma, Konstantin Androsov, Jan Steggemann, Leonardo Cristella, Roberto Castello, Alessandro Degano, Mingkui Wang, Zhirui Xu, Chao Wang, João Miguel das Neves Duarte, Tian Cheng, Yixing Chen, Werner Lustermann, Andromachi Tsirou, Alexis Kalogeropoulos, Andrea Rizzi, Ioannis Papadopoulos, Paolo Ronchese, Thomas Muller, Ho Ling Li, Giuseppe Codispoti, Hua Zhang, Siyuan Wang, Peter Hansen, Daniel Gonzalez, Tao Huang, David Vannerom, Paul Turner, Ji Hyun Kim, Donghyun Kim, Dipanwita Dutta, Zheng Wang, Sanjeev Kumar, Wei Li, Yong Yang, Geng Chen, Yi Wang, Ajay Kumar, Ashish Sharma, Georgios Anagnostou, Joao Varela, Csaba Hajdu, Muhammad Ahmad, Ekaterina Kuznetsova, Ioannis Evangelou, Matthias Weber, Muhammad Shoaib, Milos Dordevic, Vineet Kumar, Vladimir Petrov, Francesco Fiori, Quentin Python, Meng Xiao, Hao Liu, Sourav Sen, Yanlin Liu, Viktor Khristenko, Marco Trovato, Gurpreet Singh, Fan Xia, Kai Yi, Bibhuprasad Mahakud, Zhen Liu, Lei Feng, Muhammad Waqas, Shuai Liu, Hui Wang, Seungkyu Ha, Davide Cieri, Maren Tabea Meinhard, Giorgia Rauco, Aram Avetisyan, Ali Harb, Benjamin William Allen, Renjie Wang, Charles Dietz, Alexandre Aubin, Xin Sun, Juan Ramon Castiñeiras De Saa