Metal-Based Chemosensors for Important Bioanalytes
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The synthesis of water-sol., organometallic macrocycles is described. They were obtained by self-assembly in reactions of the half-sandwich complexes [{Ru(C6H5Me)Cl2}2], [{Ru(p-cymene)Cl2}2], [{Rh(Cp)Cl2}2], and [{Ir(Cp*)Cl2}2] with the ligand 5-dimethylam ...
The reaction of half-sandwich complexes of ruthenium, rhodium, and iridium with amino-substituted 3-hydroxy-2-pyridone ligands in aqueous solution gives monomeric O,O'-chelate complexes. Upon addition of base, the complexes assemble to form trimeric metall ...
Motivated by recent developments concerning coloration and energy storage in lithium intercalated nanostructural TiO2, quantum chem. Hartree-Fock calcns. have been carried out to study lithium atom intercalation in rutile and anatase. Equil. geometries and ...
A future fusion reactor will use deuterium and tritium as fuel. The former is found in abundance in seawater, while the latter is not available naturally due to its short lifetime. Present developments in the context of fusion propose generating tritium in ...
The reaction of FePS3 single crystals with a 1.6M n-butyl lithium solution in n-hexane has been followed through de electrical conductivity measurements as a function of the intercalation time. In order to investigate the influence of lithium insertion on ...
This paper present a polarimetric fiber optics current sensor using a 22.5 degree Faraday rotator and a Faraday rotation mirror. The objective of this sensor is to be low-cost, high accuracy and easy to manufacture ...
Society of Photo-Optical Instrumentation Engineers1999
Reaction of Ph3P+C-HR with R1CHO at -78 Deg yielded Ph3P+CHRCHR1O- (I). Subsequent addn. of BuLi gave Ph3P+C-RCHR1O- Li+ (II). Reaction of II with HCl and hydrolysis with tert-BuOK gave .apprx.80% RCH:CHR1 (R = Et, Ph, or C5H11; R1 = Me, Et, or C5H11). Whe ...
Alternative cathode materials were investigated for application to high voltage lithium ion batteries. Manganese based materials were considered due to the low cost and environmentally sustainable impact. Layer-structured oxide and phospho-olivine material ...
There is considerable interest in synthetic ionophores with high affinity and selectivity for Li+. But so far, compounds that selectively bind Li+ in the presence of other alkali and alkaline earth metal ions are rare and current approaches toward this goa ...
Intercalation of lithium ions in nanoporous anatase TiO2 was studied with XPS using a novel electrochem. prepn. technique. The electrolyte was 0.5 M LiClO4 in acetonitrile (not water-free). The electrochem. insertion of lithium ions creates reduced Ti ions ...
