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Laser frequency combs are coherent light sources that emit a broad spectrum of discrete, evenly spaced narrow lines whose absolute frequency can be measured to within the accuracy of an atomic clock. Their development in the near-infrared and visible domai ...
Be it to aerate a glass of wine before tasting, to accelerate a chemical reaction or to cultivate cells in suspension, the “swirling” (or orbital shaking) of a container ensures good mixing and gas exchange in a simple and intuitive way. Despite being used ...
Slurries are often used in chemical and pharmaceutical manufacturing processes but present challenging on-line measurement and monitoring problems. In this paper, a novel multivariate kinetic modeling application is described that provides calibration-free ...
Reflection absorption infrared spectroscopy (RAIRS) was used to probe for vibrational bond-selectivity in the dissociative chemisorption of three partially deuterated methane isotopologues on a Pt(111) surface. While a combination of incident translational ...
A micromirror array composed of 2048 silicon micromirrors measuring 200 x 100 mu m(2) and tilting by 25 degrees was developed as a reconfigurable slit mask for multi-object spectroscopy (MOS) in astronomy. The fill factor, contrast, and mirror deformation ...
The development of nanostructured materials with predictable and controllable connectivity and functionalities has sparked a multitude of research directions. We have been studying emerging metal-org. framework (MOFs) systems aimed at applications that ben ...
In this thesis, I describe the design and first applications of a new molecular-beam/surface-science ultra-high vacuum apparatus. The new machine combines rovibrational state-selective infrared pumping of gas-phase reactants with reflection absorption infr ...
The use of Process Analytical Technology (PAT) recommended by the Food and Drug Administration (FDA) has significantly increased during the past years in the design, control and monitoring of pharmaceutical or chemical manufacturing processes. Nowadays, PA ...
The mechanism of formation of rhodium nanocubes in the presence of tetradecyltrimethylammonium bromide and polyvinylpyrrolidone in ethylene glycol was studied in situ by XAFS, in conjunction with other ex situ techniques including MALDI-TOF MS, XRD, TEM, a ...
Changes in the colloid-chemical and photocatalytic properties of titania nanoparticles by attrition milling in the presence of glycine (Gly) and subsequent heat treatment were examined. By milling at 1500 rpm for 6 h, the average particle size was decrease ...
