Synthesis, crystal structure, and electrochemical properties of Ni(II) and Cu(II) complexes with two unsymmetrical N2O2 Schiff base ligands
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The ternary sulfide Ag7TaS6 displays high Ag-ion conductivity at ambient temperature, and the framework TaS6 and Ag ions can be respectively regarded as the host structure and guest ions. Two low-temperature phases, i.e. Ag7TaS6 II and Ag7TaS6 III, were fo ...
The crystal structure of the new synthetic compound Ba-5[B20O33(OH)(4)] . H2O was established by the methods of X-ray diffraction (a Stoe IPDS diffractometer, lambda MoKalpha, 1860 independent reflections, anisotropic refinement, R = 1.95%, localization of ...
Norbornene and norbornadiene insert across the exo-face of their C=C bond into the Pd-acyl bond of [(OC)(3)Fe{mu-Si(OMe)(2)(OMe)}(mu-dppm)Pd{C(=O)Me}] and (1a) (dppm = Ph2PCH2PPh2) to afford the heterodinuclear complexes [(OC)(3){(MeO)(3)Si}Fe(mu-dppm)Pd{C ...
The trigonal structure of a new member of the eudialyte group was established from X-ray single-crystal diffraction, lambda(MoKalpha) = 0.71073 Angstrom; space group R3m; a = 14.153(9) Angstrom, c = 60.72(5) Angstrom, V = 10546.1 Angstrom(3); M = 3050; D-x ...
Single crystals of GaInTe2 were grown from a melt and characterized by various experimental techniques, such as x-ray diffraction, x-ray photoelectron spectroscopy (XPS), and electrical and photoluminescence (PL) measurements. Our investigation evaluated i ...
The reactions of lithium and sodium aluminum hydride with alcs. and phenols in ether solvents were studied as a route to mono-, di- and triorganyloxyhydridoaluminates MAlH4-n(OR)n. However, the stability of these compds. towards disproportionation is stron ...
GalnSe(2) single crystals have been grown and characterized by experimental techniques such as high-resolution transmission electron microscopy, x-ray diffraction, x-ray photoelectron spectroscopy and optical and electrical measurements. The samples were p ...
Combined X-ray absorption spectroscopy (XAS) and X-ray diffraction (XRD) experiments have been carried out on alpha-GaAsO4 (berlinite structure) at high pressure and room temperature. XAS measurements indicate four-fold to six-fold coordination changes for ...
At -20 degrees C, SO2 undergoes homocheletropic addition with 7,7-dimethyl[2.2.1]hericene (18) to give (1R,5S)-6,10-dimethylidene-8-isopropylidene-3-thiatetracyclo[5.2.1.0(1,5 ).0(5,9)]decane 3,3-dioxide (21). This 3,3-dioxide (21). This sulfolane Is isome ...
The determination of the crystal structure of the bacterial protein proaerolysin provided the first view of a pore-forming toxin constructed mainly from beta-sheet. The structure that was obtained and subsequent crystallographic and biochemical studies hav ...
