Analysis of two-dimensional nuclear magnetic resonance spectra with relayed proton-proton-carbon magnetization transfer: a step toward automated structure elucidation
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H-1-detected solid-state nuclear magnetic resonance (NMR) experiments are recorded on both intact and trypsin-cleaved sedimented measles virus (MeV) nucleocapsids under ultra-fast magic-angle spinning. High-resolution H-1,N-15-fingerprints allow probing th ...
We investigate the optimal implementation of windowed LG4 decoupling for the direct acquisition of high-resolution H-1 solid-state NMR spectra in the moderate magic-angle spinning regime ((r)
PROBLEM TO BE SOLVED: To provide an effective and speedy method for decoupling of homonuclear couplings.SOLUTION: This invention concerns a method for high resolution NMR (nuclear magnetic resonance) measurements comprising the application of excitation pu ...
A method for nuclear magnetic resonance (NMR) spectroscopy of a sample comprises preparation of the sample and carrying out an NMR spectroscopy measurement. Preparation includes excitation of long lived coherences (LLC) between the singlet state S0 and the ...
We present two sequences which combine (H-1,N-15) and (N-15,C-13) selective cross-polarization steps with an efficient variant of the J-based homonuclear transfer scheme, in which a spin-state-selective ((SE)-E-3) block is incorporated to improve both reso ...
Heteronuclear lanthanide terephthalate coordination polymers with the general chemical formula [Ln2-2xLn2x(bdc)3(H2O)4], for which bdc2- symbolizes benzene-1,4-dicarboxylate (or terephthalate) and Ln and Ln represent trivalent rare earth ions, were synthes ...