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The performance of deuterium-carbon correlation (DECOR) spectroscopy for the assignment and measurement of deuterium quadrupolar couplings in fully deuterated liquid crystalline phases is analyzed. The experiment relies on a broadband polarization transfer ...
The aminophosphine C6H4(o-CN)NHPPh2, 1, containing an electron-withdrawing nitrile group, was prepared from the lithiation of 2-aminobenzonitrile followed by addition of Ph2PCl. Lithiation of 1 using (BuLi)-Bu-n affords the anion [Ph2PN(Li)C6H4(o-CN)(thf)] ...
The authors present measurements of the temperature dependence of the RF penetration depth δ(T) in YBa2Cu3O6.9 and BiSrCaCu2Ox ceramics. They found that δ(T) closely follows the Gorter-Casimir two-fluid model at T
The methanol dehydration reaction was studied over environmentally benign, easily accessible and inexpensive K10 montmorillonite clay used as the catalyst at a temperature range between 200–700 °C. Nearly 100% selectivity towards dimethyl ether (DME) at 80 ...
The apparatus according to the invention comprises a coupler (30) intended to couple between each other two monomode fibres presenting four branches (31, 32, 33, 34). The branch (31) is connected to a branch (36). The branch (33) is the reference fibre and ...
We present the design, fabrication and test of high-Q factor radiofrequency planar microcoils for nuclear magnetic resonance (NMR) spectroscopy in small volume samples. The coils are fabricated on glass wafers using high-aspect ratio SU-8 photoepoxy and co ...