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A dense post-rutile titanium dioxide (TiO2) phase was discovered in shocked garnet gneisses from the Ries crater by reflected-light microscopy, laser rnicroRaman spectroscopy and micro-beam X-ray diffraction. The Raman spectrum consists of nine bands at wa ...
Electron crystallography and atomic force microscopy allow the study of two-dimensional membrane protein crystals. While electron crystallography provides atomic scale three-dimensional density maps, atomic force microscopy gives insight into the surface s ...
High-resolution transmission electron microscopy (HRTEM), electron microdiffraction, and X-ray diffraction were used to study hydroxyapatite specimens with particle sizes from a few nanometers to several hundreds of nanometers. Diffuse scattering (without ...
Calcium phosphate precipitation obtained from aqueous solutions at room and body temperatures and pH 5.5-7.5 were investigated by high-resolution transmission electron microscopy (HRTEM), transmission electron diffraction, scanning electron microscopy (SEM ...
The low temperature (LT) modification of Cs3Bi2I9 has been refined to R(F) = 0.055 on the basis of X-ray diffraction measurements at T = 130 K from a twin crystal with six fractions connected by 3-fold axis and m-planes symmetry operations. Data were colle ...
Structure and morphology of solid particles in precipitation from aqueous solutions correlate with formation (solution) conditions and thus reflect the growth mechanism. Calcium phosphate precipitation obtained from dilute aqueous solutions at room and bod ...
The structure of Cs3Bi2I9 has been refined to R = 0.0165 on the basis of X-ray diffraction measurements at T = 290 K (STOE IPDS diffractometer; MoKalpha-radiation; 296 nonequivalent reflection with I > 2 sigma(I)). The absorption correction was accounted f ...
The high- and low-temperature forms, i.e., phase I (stable above 328 K) and phase II (stable below 328 K), of Cu8GeSe6 have been investigated by the powder X-ray diffraction method. Cu8GeSe6 II is hexagonal with A = 12.6438(2), C = 11.7570(1) Angstrom, Z = ...
Since the discovery of X-ray diffraction, it was believed that the discrete distribution of diffracted intensities was a direct consequence of the periodic arrangement of atoms in the three dimensions of space. However, in the last thirty years many exampl ...
Incommensurate structure of Hexamethylenetetramine suberate (C6H12N4)(HOOC-(CH2)6-COOH) has been solved from single crystal x-ray diffraction data. A molecular dynamics simulation of this system was carried out from 15 K to 580K. A second-generation consis ...