Nuclear magnetic resonance spectroscopy of proteins
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By applying a variational principle on a magnetic system within the framework of extended irreversible thermodynamics, we find that the presence of a temperature gradient in a ferromagnet leads to a generalisation of the Landau-Lifshitz equation with an ad ...
Some triphenyltin(IV) adducts with a family of diphosphoryl ligands, RR'P(O)-X-P(O)RR' (R = OPh, Ph, R' = R, An (aniline)) and X = 1,4-OC6H4O, 1,4-OC6H4NH, 1,4-NHC6H4NH 1,4-(NHCH2)(2)C6H4, 1,3-(NHCH2)(2)C6H4 and piperazine have been synthesized and charact ...
H-1 NMR has been used to characterise white Portland cement paste incorporating 10 wt.% of silica fume. Samples were measured sealed throughout the hydration without sample drying. Paste compositions and C-S-H characteristics are calculated based on H-1 NM ...
The interaction between the endohedral unit in the single-molecule magnet Dy2ScN@C-80 and a rhodium (111) substrate leads to alignment of the Dy 4f orbitals. The resulting orientation of the Dy2ScN plane parallel to the surface is inferred from comparison ...
A series of novel polysiloxanes is presented, the glass transition temperatures and dielectric properties of which are systematically fine-tuned by utilizing thiol-ene post-polymerization reactions. The pendant vinyl groups of a high molecular weight polym ...
From epidemiological studies it is known that diabetes patients display increased risk of developing dementia. Moreover, cognitive impairment and Alzheimer's disease (AD) are also accompanied by impaired glucose homeostasis and insulin signalling. Although ...
Vinyl end-functionalized polysiloxanes P-x containing varying mol% of trifluoropropyl groups (x) were prepared starting from 1,3,5-tris(3,3,3-trifluoropropyl)-1,3,5-trimethylcyclotrisiloxane (F-3) and octamethylcyclotetrasiloxane (D-4) via anionic polymeri ...
The human voltage dependent anion channel 1 (VDAC) is a 32 kDa β-barrel integral membrane protein that controls the transport of ions across the outer mitochondrial membrane. Despite the determination of VDAC solution and diffraction structures, a structur ...
A strong spin-orbit interaction leads to a Rashba-type splitting of the bulk bands of BiTeCl, which results in toroidal Fermi surfaces with distinct spin structures depending on the chemical potential. Here, we present spin-and angle-resolved photoelectron ...
The use of small rotors capable of very fast magic-angle spinning (MAS) in conjunction with proton dilution by perdeuteration and partial reprotonation at exchangeable sites has enabled the acquisition of resolved, proton detected, solid-state NMR spectra ...
