Chromatographie en phase gazeuse-spectrométrie de masse
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Reversed-phase HPLC can not be relied on as the only chromatog. step for the purifn. and anal. of synthetic peptides larger than 30 to 40 residues; therefore their purity should be documented by more than one anal. technique. Narrow-bore ion-exclusion chro ...
To obtain addnl. insight into the release mechanism of the metals in electrothermal atomization at. absorption spectrometry, a quant. relation between the heat of vaporization and the size of the released particles is proposed from the Kelvin equation. The ...
Controversy regarding the interpretation of photoionization efficiency measurements obtained for alkali clusters provided impetus for higher-resoln. (3.3 nm) studies . The new data cover the full range of cluster sizes: Nax, x
Periodic operation was applied to the CO2 methanation reaction at 383 K on 2% Ru/TiO2. A continuous feed recycle reactor combined with a diffuse reflectance infrared cell and a mass spectrometer allowed to follow simultaneously the gas phase CO2 and CH4 as ...
In this paper we present the first results obtained with a plasma ion mass spectrometer in the boundary of the TEXTOR tokamak. Measurements were made several days after TEXTOR was boronised. Comparisons are made with results obtained in DITE under similar ...
Negative ions have been clearly identified in silane rf plasmas used for the deposition of amorphous silicon. Mass spectra were measured for monosilicon up to pentasilicon negative ion radical groups in power-modulated plasmas by means of a mass spectromet ...
Methods and spectrometers for carrying out ion-cyclotron-resonance spectrometry are described in which a pulse sequence is employed which is described by P1-t1-P2-Tm-P3-t2, (P1, P2, and P3 are radio-frequency pulses, with P1 and P2 having the same frequenc ...
On-column thermooptical absorbance (TOA) detection in capillary electrophoretic separations of various nucleoside and mono- and diphosphate nucleotide mixtures absorbing at 257 nm is demonstrated in 20 μm i.d. capillaries. The analytes are optically pumped ...
To overcome ammonia inhibition in animal cell culture, a method utilizing porous polytetrafluoroethylene membranes with an assocd. pH gradient was investigated. Model expts. without cells were carried out in three different reactor configurations suitable ...
The time-resolved fluxes of negative polysilicon hydride ions from a power-modulated rf silane plasma have been measured by quadrupole mass spectrometry and modeled using a simple polymerization scheme. Experiments were performed with plasma parameters sui ...
