Solidification Behaviour of PLLA/nHA Nanocomposites
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This paper describes the synthesis of two novel tetra 2-bromoisobutyric acid-substituted perylene fluorophores and their use as initiators for the atom transfer radical polymerization of styrene. Different star-shaped polystyrenes covering a wide range of ...
In addn. to online detection of events in biotechnol., calorimetry could be used to control processes. In the latter case, a correct and instantaneous heat signal must be available. This would be possible only if a correct evaluation of baseline evolution ...
The curing reaction of an epoxy resin [diglycidyl ether of bisphenol A (DGEBA)] combined with a methyl-hexahydrophtalic anhydride (MHHPA) hardener and a benzyldimethylamine (BDMA) accelerator was studied over a temperature range of 60140°C to build its is ...
Two novel tetra- and hexahydroxy functionalized perylene chromophores have been used as initiators for the Sn(oct)2 catalyzed ring-opening polymerization of different lactones. The arms of the resulting star polymers were comprised of either crystallizable ...
Bench-scale heat flux calorimetry is applied to monitor complex microbial systems producing secondary metabolites and having a rheol. complex behavior. With such systems, biol. metabolic activity can only be measured accurately if calorimetry is improved b ...
Transformations of the quasi-crystalline icosahedral phases formed in the melt-spun AlMn(Si) alloys Al90Mn10, Al86Mn14 and Al75Mn20Si5 have been studied at high temperatures (300-1000 K) by combined measurements of resistivity, differential scanning calori ...
The kinetic properties of the Me methacrylate (MMA) polymn. at pilot scale for a given temp. range (130-170 Deg) were detd. by differential scanning calorimetry and batch expts. reflecting initiation by MMA peroxides, depropagation of the living chains as ...
Reaction calorimetry is an efficient tool used to obtain kinetic, thermodn. and safety data. A reaction calorimeter, RC1e-HP350, developed in collaboration with Mettler-Toledo GmbH, allows investigating chem. reactions under supercrit. conditions. The main ...
Calorimetry (adiabatic, isothermal, differential, oscillating or acoustic) is generally based on heat-flow measurements of the studied system. Most of its applications are dedicated to kinetic-parameter detn., safety studies and process optimization, phase ...
The crystallization kinetics of polyamide-12 has been investigated using a combination of differential scanning calorimetry (DSC) and hot-stage optical microscopy. The DSC data for isothermal crystallization were consistent with a simple two-parameter Avra ...