Electron paramagnetic resonance magnetic field sensors for particle accelerators

Anthony Jean Beaumont, Giovanni Boero, Marco Buzio, Alessandro Valentino Matheoud
2020
Article

Résumé

We report on four electron paramagnetic resonance sensors for dynamic magnetic field measurements at 36 mT, 100 mT, 360 mT, and 710 mT. The sensors are based on grounded co-planar microwave resonators operating at about 1 GHz and 3 GHz, realized using printed circuit board technology, and on single-chip integrated microwave oscillators operating at about 10 GHz and 20 GHz, realized using complementary metal-oxide-semiconductor technology. The sensors are designed to mark precisely the moment when a time-dependent magnetic field attains a specific value. The trigger from the sensor can be used to preset the output of real-time magnetic field measurement systems, called "B-trains," which are in operation at several large synchrotron installations, including five of the CERN's particle accelerators. We discuss in detail the performance achieved, in particular, the magnetic field resolution that is in the range of 0.1 nT/Hz(1/2)-6 nT/Hz(1/2). The effects of material anisotropy and temperature are also discussed. Finally, we present a detailed characterization of the sensors with field ramps as fast as 5 T/s and field gradients as strong as 12 T/m.

Official source

https://infoscience.epfl.ch/record/281178?ln=fr

À propos de ce résultat

Cette page est générée automatiquement et peut contenir des informations qui ne sont pas correctes, complètes, à jour ou pertinentes par rapport à votre recherche. Il en va de même pour toutes les autres pages de ce site. Veillez à vérifier les informations auprès des sources officielles de l'EPFL.

Concepts associés

Chargement

Publications associées

Chargement

Ferrimagnetic resonance field sensors for particle accelerators

Anthony Jean Beaumont, Giovanni Boero, Marco Buzio

We report on two ferrimagnetic resonance (FMR) sensors for absolute dynamic magnetic field measurements at 36 and 100 mT. The sensors are designed to mark precisely and reproducibly the moment when a time-transient magnetic field attains a specific value. The trigger from the sensor can then be used for real-time magnetic field measurement systems, called B-trains, which are in operation at several large synchrotron installations including five of CERN's particle accelerators. We discuss in detail the design, the operation, and the performance of the FMR sensors based on two different types of printed circuit board (PCB) resonator structures.

AMER INST PHYSICS2019

Chargement

Electron Spin Resonance Magnetometers for Particle Accelerators

Anthony Jean Beaumont

CERN is the European Organization for Nuclear Research located in Geneva, Switzerland. Its main goal is to explore fundamental physics and it exists primarily to provide physicists the necessary tools for doing this, namely accelerators. These tools bring particles to almost the speed of light and then use them in different experiments. The CERN Accelerator Complex includes a chain of interconnected accelerators allowing the acceleration of charged particles up to 6.5 TeV per beam (for protons) in 2018 by the Large Hadron Collider (LHC). Different types of accelerator exist, but at CERN the most common are the synchrotrons. For those, the magnetic field is synchronous with the beam momentum. Magnetic models cannot be always used to predict the field within the required reproducibility, which may be as low as 10^(-5), due to non-linear effects (eddy currents, saturation and hysteresis). Therefore, most of the CERN's synchrotrons are equipped with a real time magnetic field measurement system, the so called "B-Train". The magnetic field measurement devices are composed of absolute field sensors (called "markers"), field tracking sensors (called "induction coils"), an acquisition system, a control system that calculates the magnetic field from the sensors, and a distribution system that delivers the field value to the users. Due to the configuration of the CERN accelerator chain, if one of the injectors fails, the LHC cannot have beam. Consequently, a huge consolidation program of the real time magnetic measurement systems was launched to guarantee operation in the long term. Thus the markers are critical devices for operations at CERN and must be carefully developed to fulfil the high performance and reliability requirements of the B-Train systems. This thesis propose new designs for electron spin resonance (ESR) field markers. We discuss in details the design, the operation, and performance of the ESR sensors based on resonator and oscillator structures including comparison between paramagnetic and ferrimagnetic samples. We propose four field marker levels at 36 mT, 106 mT, 360 mT and 710 mT that correspond to resonance frequencies of 1GHz, 3GHz, 10GHz and 20 GHz. Those measurement values cover most of the marker level requirements of the CERN accelerators and achieving resolution up to 0.1 nT/Hz^(1/2) for field ramps as fast as 5 T/s and field gradients as strong as 12 T/m. We conclude with measurements validation performed on the Proton Synchrotron (PS) and on the Low Energy Ion Ring (LEIR) accelerators.

EPFL2020

Chargement

Scanning probe microscopy has become, nowadays, a branch of microscopy widely used to image surfaces of different specimens. Among the various applications, the magnetic imaging is one of the most exciting scanning probe microscopy techniques. It allows the study of topography of samples at the nanometer scale. The magnetic force microscopy is the best known and the most employed magnetic imaging technique. It has been successfully used for the imaging of various samples but with the major inescapable limitations that it is confined to the surface, non-quantitative and invasive. Techniques such as the scanning Hall probe microscopy (SHPM) and the magnetic resonance force microscopy (MRFM) have emerged, several years later, as promising approaches to overcome these limitations. In this thesis, we present the design, the fabrication and the characterization of, first, micro-Hall sensors on SU-8 cantilevers used for SHPM and, second, of ultrasensitive Si cantilevers used for MRFM experiments. A microfabrication technique has been developed to produce hybrid devices consisting of micro-nano Hall sensors integrated on SU-8 cantilevers. Two materials have been used to produce the Hall sensors. First, bismuth (Bi) was chosen for its low carrier charge density and its negligible surface charge depletion effects so that it should provide sensitive sensors. The second material tested was nickel (Ni), chosen for the dominant effect called the extraordinary Hall effect. The active areas of 5×5, 2×2 and 1×1 µm2 were realized and reproduced with the standard photolithography. Producing submicron Hall sensors required the use of the focused ion beam (FIB) that allowed a decrease of the size of the sensors down to 80×80 nm2. The delicate transferring of the nano sensors on the polymer cantilevers was successful. Bi micro-Hall sensors have shown a fragility making them delicate to handle. However, the Ni micro-Hall sensors had an excellent functionality. Their characterization has shown sensors with a low sensitivity compensated by the high applied current providing a high magnetic field resolution. The magnetic field images were carried out using the Ni micro-Hall sensors. They had a high stability during the imaging experiments. The spatial resolution was set by the sensors active area limited to the micro-meter scale. However, the magnetic field resolution is better than 1 T/√Hz a result comparable to the high resolution offered by the semiconductors. Single crystal silicon cantilevers have been fabricated for use in MRFM experiments. Also, cantilevers with integrated micro-magnets have been successfully produced. The developed microfabrication technique has allowed a high yield production (up to 70%). The softest fabricated cantilevers are 0.34 µm thick, 500 µm long and 10 µm wide. These cantilevers have been characterized under vacuum conditions (1×10-6 mbar). The resonance frequencies and the quality factors were measured using the frequency sweep or noise methods and both provided the same results. The Rayleigh method that we have adapted to the cantilevers geometry, made it possible to estimate the theoretical resonance frequencies with a good approximation and the calculated values fit well with the measured ones. All the cantilevers have a quality factor above 20000 and the force sensitivity achieved was between 10-16 and 10-17 N/√Hz A mathematical model has been developed based on the motion equation of a harmonic oscillator under the influence of a magnetic field. The model was studied to find the expression of the resonance frequency of cantilevers with integrated magnetic tips in the presence of a parallel or a perpendicular magnetic field. The shift in frequency due to the presence of the applied magnetic field depended on the magnetic tip magnetization. The measurement of the frequency shift should permit the calculation of the magnetization of these micro-magnets directly integrated on the cantilevers. The probes that we have realized represent micro and nano tools suitable for the magnetic field imaging that can be done with the SHPM and MRFM techniques.

EPFL2007

Chargement

Electron Spin Resonance Magnetometers for Particle Accelerators

Anthony Jean Beaumont

EPFL2020

EPFL2007