High-dimensional parameter determination based on mr fingerprinting measurements
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We present the design, fabrication and test of high-Q factor radiofrequency planar microcoils for nuclear magnetic resonance (NMR) spectroscopy in small volume samples. The coils are fabricated on glass wafers using high-aspect ratio SU-8 photoepoxy and co ...
New 2-dimensional NMR correlation methods are presented which allow one to obtain selected high-resoln. multiplets where all signals have pos. pure absorption peak shapes. The multiplets do not suffer from any cancellation effects, and their fine structure ...
The performance of deuterium-carbon correlation (DECOR) spectroscopy for the assignment and measurement of deuterium quadrupolar couplings in fully deuterated liquid crystalline phases is analyzed. The experiment relies on a broadband polarization transfer ...
This paper presents the results of the investigation of the hydration of alkali-activated slag (AAS) by nuclear magnetic resonance spectroscopy (NMR). The cross-polarization (CP) technique was used in combination with magic-angle spinning (MAS). This resea ...
Selective single-transition cross-polarization (ST-CP) may be achieved in four-level systems such as encountered in NMR of scalar-coupled two-spin systems (for example, 15N-1H groups in peptides), by employing two selective resonant fields applied to a pai ...
An ultrashort-echo-time stimulated echo-acquisition mode (STEAM) pulse sequence with interleaved outer volume suppression and VAPOR (variable power and optimized relaxation delays) water suppression was redesigned and optimized for human applications at 4 ...
In this thesis, the synthesis of oligomers of β-amino acids (β-peptides) is described. Their secondary structure is investigated by several techniques, in particular nuclear magnetic resonance (NMR) spectroscopy, but also circular dichroism and infrared sp ...
Homonuclear proton-proton coupling consts. can be detd. accurately by recording selective two-dimensional correlation spectra and by analyzing the resulting multiplets by two-dimensional convolution and deconvolution methods. These methods were evaluated b ...
New NMR techniques are described for transferring transverse magnetization between scalar-coupled nuclei in the rotating frame. The methods involve simultaneous spin-locking of two selected spins A and X, using cosinusoidal modulation of the radio frequenc ...
NMR spectroscopy is one of the newer spectroscopic techniques for investigating the static, dynamic and electronic structures of molecules adsorbed onto metal catalyst surfaces. We review recent progress in the application of solid-state NMR methods to the ...