Extreme temperature sensing using Brillouin scattering in optical fibers

Stimulated Brillouin scattering in silica-based optical fibers may be considered from two different and complementary standpoints. For a physicist, this interaction of light and pressure wave in a material, or equivalently in quantum theory terms between photons and phonons, gives some glimpses of the atomic structure of the solid and of its vibration modes. For an applied engineer, the same phenomenon may be put to good use as a sensing mechanism for distributed measurements, thanks to the dependence of the scattered light on external parameters such as the temperature, the pressure or the strain applied to the fiber. As far as temperature measurements are concerned, Brillouin-based distributed sensors have progressively gained wide recognition as efficient systems, even if their rather high cost still restricts the number of their applications. Yet they are generally used in a relatively narrow temperature range around the usual ambient temperature; in this domain, the frequency of the scattered light increases linearly with the increase in temperature. The extension of this range toward higher (up to 800°C) and lower (down to 1 K) temperature is the main aim of this thesis. In both cases, our measurements on various fiber samples show that the aforementioned linearity does not hold. Most notably, the characteristics of Brillouin scattering at low and very low temperature are strikingly different from those observed under normal conditions; they are directly related to the disordered nature of the silica that constitutes the fiber, what motivates the large place we here devote to the physics of amorphous solids. Despite the observed nonlinearities, our results demonstrate the feasibility of thermometry based on Brillouin scattering over the full investigated temperature range. We can thus swap in the last part of this work the physicist's point of view for that of an engineer and present the setup and the performances of a sensor, or rather of a whole family of sensors we have tested and improved in the course of the last few years; moreover, some real measurement examples are given. Finally, we propose some possibilities of further enhancement, that remain right now at the preliminary stage of their development.

La diffusion Brillouin dans les fibres optiques

Among all non-linear optical effects observed in single-mode optical fibres, stimulated Brillouin scattering (SBS) is of particular importance since it has numerous practical implications. SBS occurs when laser waves are scattered through the interaction of light with hypersonic acoustic waves in the medium. It manifests through the generation of a backscattered Stokes wave that carries most of the input optical power once a definite intensity level is reached within the fibre core. It limits the maximum optical power that can be transmitted through an optical fibre and therefore can cause a severe penality for fibre optics telecommunications. The backscattered Stokes wave is down shifted in frequency with respect to the incident lightwave frequency. This frequency shift – often called the Brillouin frequency shift – depends on the fibre parameters and on the wavelength of the incident light. It is directly proportional to the acoustic velocity and ranges from 12 to 13 GHz for silica fibres at a 1.3 µm wavelength. The Brillouin frequency shift is also very sensitive to environmental quantities changing the acoustic velocity such as temperature and strain. This feature makes SBS very interesting for temperature and strain monitoring in optical fibres and has been used in the design of fibre optics sensors. In the present work, a novel method to measure SBS characteristics in single-mode optical fibres has been developed. It is based on the so-called pump and probe technique using two counterpropagating optical waves within the test fibre. It basically presents the originality to require only one laser source and relies on an electro-optic modulator to generate the probe signal by microwave modulation of the pump light. The inherent high stability of the experimental set-up has made possible the characterisation of different fibres in terms of SBS parameters with a higher accuracy than the traditional two lasers set-up. The influence of dopant concentration in silica fibres on the SBS properties has been fully characterised. Furthermore it has been determined that the presence of core dopants decreases the acoustic velocity resulting in a smaller Brillouin frequency shift. The temperature and strain effects on the SBS characteristics have been extensively investigated. The problem of the evolution of the polarisation of the interacting lightwaves has been studied and a model clarified the so far unexplained behaviour in low birefringence fibres. A new measurement procedure has been defined to achieve polarisation-independent Brillouin gain determination. The second facet of the present thesis deals with the concept of distributed fibre optics sensors based on SBS. The determination of the Brillouin frequency shift gives access to the temperature or strain experienced by the fibre, while a modified OTDR technique provides the information on the position. Here again the use of a single laser source together with an electro-optic modulator brings several advantages. Besides the convenient flexibility in the generation of the probe signal, it makes possible to pulse the optical signals to localise the interaction within the test fibre. The overall temperature or strain distribution of the test fibre can be carried out by measuring the Brillouin frequency shift at any locations throughout the test fibre. A sensor has been experimentally achieved and its performances can be summarised as follow: spatial resolution less than 10 meters over more than 10 kilometres, with a resolution on the Brillouin frequency determination of 1 MHz, that corresponds to a ±1°C temperature resolution or to a 2x10-5 strain resolution. The dynamic range can be increased up to 30 kilometres to the detriment of the spatial resolution. The ultimate performances of the SBS distributed fibre optics sensors have been investigated in terms of spatial resolution and dynamic range. It turns out that these sensors are eventually dedicated to distributed measurements over several tens of kilometres with a spatial resolution limited to the meter range. Finally two practical applications of such sensors are described: the measurement of the strain distribution in installed fibre optics cables for telecommunications and the temperature monitoring of electrical energy distribution cables. On site measurements using a Brillouin sensor have been performed for the first time thanks to the high stability and reliability of the sensor.

EPFL1997

Construction material monitoring with "optical hair" hygrometers

Pascal Kronenberg

Moisture is an essential parameter in the behaviour of capillary-porous construction materials such as timber and concrete. It affects liquid and gas transport phenomena, chemical and biological degradation processes, mechanical properties and, in the case of concrete, hydration. From a scientific point of view, moisture monitoring is essential in order to improve the understanding of material behaviour. Moisture measurements may increase the predictive accuracy of established material behaviour models. In practice, the increased knowledge of material behaviour improves structural maintenance planning. The main objective of this work is to propose a measurement method for non-destructive, in-depth moisture monitoring of construction materials. In this context, an intrinsic point and an averaging fibre optic relative humidity sensor have been developed and tested. The sensors are based on optical fibres that are coated with a hygroscopically swelling transducer polymer. When wet, the swelling of the coating strains the fibre (analogy with the hair hygrometer). The induced strain is assessed with conventional fibre optic strain sensing techniques such as fibre Bragg gratings and Michelson interferometry. Theoretical and experimental studies lead to a detailed understanding of the influence of humidity and temperature on the steady and transient state sensor behaviour. The sensors have an accurate, linear, reversible and reproducible response to relative humidity between 5 and 95 %RH and between 13 and 60 °C, at least. The sensor response time is in the order of 20 minutes. However, when packaged, the sensor responds slower. The temperature cross-sensitivity of the fibre Bragg grating sensor may be compensated with an additional non-hygroscopic grating, while the Michelson interferometric sensor provides an auto-compensation of temperature effects. Tests in mortar and timber samples demonstrate that the sensors preserve their sensing ability when embedded. These tests have also clarified the multiplexing potential of fibre Bragg gratings for forming a multi-point RH sensor. Multi-point sensors are particularly useful for profile measurements.

EPFL2003

Brillouin Echoes for Advanced Distributed Sensing in Optical Fibres

Stella Foaleng Mafang

Brillouin scattering is particularly efficient and attractive for the implementation of strain and temperature distributed sensing in optical fibres. Recently a trend has been observed that modern advanced applications require a substantial step towards better spatial resolution, while preserving temperature/strain precision over a long range. For this purpose the state of the art does not satisfy all these requirements. In this thesis we present a radically new approach named Brillouin Echoes distributed sensing (BEDS) that allows covering these requirements. In the first part, we propose an updated configuration of the classical existing Brillouin sensor for time domain analysis allowing drastic noise reduction. Then we investigate the limitations (due to non-linear effects) of the classical Brillouin sensor in terms of long distance range measurements. The identified nonlinear effects are pump depletion due to SBS itself, self-phase modulation (SPM), modulation instability (MI), which occurs only in fibres presenting an anomalous dispersion at the pump wavelength and Raman scattering (RS). We propose the modeling of the pump depletion effect to obtain analytical expressions that are useful for the proper design of a BOTDA sensor and for the determination of a very small depletion. The model confirmed by experimental measurements is informative on the conditions maximizing the depletion effect; therefore a standard configuration can be defined to test the value of the depletion in the set-up. Furthermore, we demonstrate that SPM-induced spectral broadening can have a significant effect on the measured effective gain linewidth. Modeling and experiments have undoubtedly demonstrated that the effective gain linewidth can easily experience a two-fold increase in standard conditions when the pulse intensity profile is Gaussian. We showed that the problem can be practically circumvented by using a clean rectangular pulse with very sharp rising and falling edges. The theoretical and experimental analysis of the undesirable effects of MI and forward RS in distributed BOTDA sensors systems gives a simplified expression to predict the critical power for a given distance range. MI turns out to be the dominant nonlinear limitation since it shows the lowest critical power, but it is less critical since it can be avoided to a wide extent by using the fibre in the normal dispersion spectral region such as a DSF in the C-band. On the other hand Raman scattering can be avoided only by limiting the optical pump power and therefore is the ultimate nonlinear limitation in a distributed sensing system. Under similar conditions RS shows a critical power ∼5 times larger than MI. In the second part, we present the new approach Brillouin echo distributed sensing (BEDS) which has proved to be a powerful solution to realize sub-metric spatial resolutions in Brillouin distributed measurements. We have demonstrated both theoretically and experimentally that an optimized configuration is reached when the optical wave is π-phase shifted. The experimental tests have shown a spatial resolution down to 5 cm, with a clear margin for further improvement down to a real centimetric spatial resolution. This optimized configuration produce the best contrast independently of the pulse intensity, with a factor 2 of improvement compared to other techniques based on the same approach (dark pulse, bright pulse). This extends the dynamic range by 3 dB, which corresponds in standard loss conditions to a 5 km extension of the sensing range. An analytical developed model has proved to be an excellent tool not only for optimizing the pumping scheme but also in post-processing the measured data. Finally the potentialities of BEDS technology provide solutions in real contexts. Using the BEDS technology in landslide monitoring at laboratory scale, for the first time it became possible to observe the failure propagation in laboratory scale with an accurate precision. Furthermore, using BEDS we have proposed and demonstrated the possibility of mapping geometrical structure fluctuations along a photonic crystal fibre (PCF). Both long- and short-scale longitudinal fluctuations in the Brillouin frequency shift have been identify and quantify. Observation of Brillouin linewidth broadening in PCF fibre through distributed measurement of the Brillouin gain spectrum using BEDS has allowed fundamental understanding of SBS in PCF fibre and in their design in view of applications to optical-strain/temperature sensing.

EPFL2011