Sub micrometer ceramic structures fabricated by molding a polymer-derived ceramic

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Liquid metal infiltration of silicon based alloys into porous carbonaceous materials Part-III: Experimental verification of conversion products and infiltration depth by infiltration of Si-Zr alloy into mixed SiC/ graphite preforms

Ludger Weber, Annapaola Parrilli, Caroline Hain, Alberto Ortona, Manoj Kondibhau Naikade

Porous carbonaceous preforms, made from graphite and silicon carbide (SiC) powders, with varying graphite powder mass fractions and particle sizes, were infiltrated at 1500 degrees C and 1700 degrees C by Si-8 at. pct Zr alloy to produce dense Si-Zr-SiC co ...

ELSEVIER SCI LTD2023

Multiscale microshaping of functionally graded polymer-derived SiCN ceramics

Lorenz Hagelüken

Polymer-derived ceramics (PDCs) exhibit excellent properties and are compatible with many shaping techniques due to the liquid character of the preceramic polymers (PCPs). Furthermore, their properties are adjustable by modifying the precursor composition ...

EPFL2022

Study and characterization of silicon metal alloys systems for the reactive infiltration process of ceramic matrix composites

Manoj Kondibhau Naikade

Silicon infiltrated silicon carbide (SiSiC) is one of the most promising and economical non-oxide ceramic matrix composites for high-temperature structural applications. In recent years infiltration by Si-alloys instead of pure Si has become popular to avo ...

EPFL2021

Additive micro-manufacturing of crack-free PDCs by two-photon polymerization of a single, low-shrinkage preceramic resin

Jürgen Brugger, Demetri Psaltis, Christophe Moser, Helena Van Swygenhoven, Eirini Kakkava, Lorenz Hagelüken, Georgia Konstantinou, Nikolaos Nianias, Jieping Wang

Additive manufacturing (AM) methods are being integrated in ceramics fabrication either as the main manufacturing tool or for auxiliary purposes. By using polymers, powders and preceramic formulated materials, AM techniques are pushing towards higher resol ...

2020

Spark Plasma Sintering of Ceramics: From Modeling to Practice

Paul Bowen, Michael Stuer, Zhe Zhao

Summarizing the work of nearly a decade of research on spark plasma sintering (SPS), a review is given on the specificities and key factors to be considered in SPS of ceramic materials, based on the authors’ own research. Alumina is used primarily as a mod ...

2020

Dynamic wetting in pressure-infiltration of ceramic particle preforms by molten metal

Gionata Schneider

This thesis investigates the interaction between mechanically induced flow of a liquid metal into a porous solid, and kinetic effects at the triple line. The approach is experimental and focuses on metal-ceramic systems for which the literature gives value ...

EPFL2019

Ni-Al2O3 nacre-like composites through hot-pressing of freeze-cast foams

A multi-step process is developed to create a nacre-like ceramic/metal composite. First, a slurry of Ni-coated alumina platelets and NiO nano-particles is directionally freeze-cast and the ice is sublimed, creating a foam with aligned lamellar walls contai ...

2019

Probing the micromechanical strength of oxide ceramic composite reinforcements

Václav Pejchal

This work shows how one can probe the micromechanical strength of ceramic reinforcements used in metal matrix composites, which greatly influences the mechanical performance of the composite material yet has seldom been quantified with precision. More spec ...

EPFL2017

Comparison of apparent activation energies for densification of alumina powders by pulsed electric current sintering (spark plasma sintering) and conventional sintering-toward applications for transparent polycrystalline alumina

Paul Bowen, Michael Stuer, Zhe Zhao, Claude Paul Carry

In the quest for high real in-line transmittances for transparent polycrystalline alumina (PCA), we need defect free processing. One of the biggest advances in producing high density defect free ceramics over recent years has been the advent of spark plasm ...

Materials Research Society2017

Strength and fracture of silicon second-phase particles in aluminium casting alloys

Martin Guillermo Mueller

The mechanical behaviour of metallic materials that have a microstructure composed of a brittle phase embedded in a ductile matrix is dictated by a complex interplay of factors such as local phase properties, cohesive properties, geometrical characteristic ...

EPFL2017

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