Ceramic Oxygen Separation Membranes and Mixed Conductors
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AbstractThe degradation of metal interconnects (ICs) in Solid Oxide Cells (SOCs) primarily results from chromium (Cr) oxide scale growth on stainless-steel substrates, causing ohmic loss and air-side electrode poisoning by Cr. This thesis addresses these c ...
Plasma nitriding was applied to ferritic stainless steel substrates to improve their performances as interconnects for solid oxide fuel cell devices. The samples underwent electrical conductivity test and SEM/EDS, TEM/EDS, environmental-SEM analyses. The f ...
2020
Solid oxide fuel cells (SOFCs) are approaching commercialization to improve power production efficiency. Currently, cost and lifetime reliability limit their spread in the market. The SOFC is ceramic-based, but refractory metal alloys are in fact the major ...
EPFL2019
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Microstructural changes in Ni–yttria stabilized zirconia (YSZ) near the YSZ electrolyte were examined by three-dimensional (3D) electron microscopy after electrolysis and fuel cell operation up to 10,700 h and 15,000 h, respectively. The depletion of Ni an ...
2020
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The performance of solid oxide cells is known to be dependent upon the density of three phase boundaries (TPB), but the potential for improving their effective electrocatalytic activity by morphological adjustments is imprecisely known. A spilling algorith ...
2019
Electron microscopy offers a wide range of techniques to study materials. Environmental Scanning Electron Microscopy (ESEM), in particular, allows the characterisation of samples at high-temperature using a laser heating stage, and under various gaseous at ...
EPFL2020
Electrochemical conversion of CO2 into useful chemicals is a promising approach for transforming CO2 into sustainably produced fuels and/or chemical feedstocks for industrial synthesis. We report that nanoporous gold (np-Au) films, with pore sizes ranging ...
2019
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Chromium evaporation is identified as a major degradation mechanism in solid oxide fuel cell (SOFC) stacks. The major chromium source is the commonly used stainless steel interconnects, thus raising a need for protective coatings on the interconnect steel. ...
2019
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The perovskite-type mixed oxide La0.3Sr0.55Ti0.95Ni0.05O3-delta (LSTN) is demonstrated to exhibit the remarkable property of structural regeneration, where Ni can be reversibly exsoluted from the host perovskite lattice resulting in a regenerable Ni cataly ...
Sputter deposited Al(1-x)ScxN thin films with a Sc content from x = 0 to 43 at% are investigated by electron microscopy in order to study and explain the formation and growth of abnormally oriented grains (AOG). It is found that the latter did not nucleate ...
