Advanced trends in nonlinear optics applied to distributed optical-fibre sensors

The distributed optical-fibre sensors based on the properties of Brillouin scattering is the central object of this thesis. In the past decade, optical fibres have gained a large interest as sensors: attractive solutions based on the non-linear stimulated Brillouin scattering have been proposed in the early 90s and the possibility to achieve long-range fully distributed strain measurements has been extensively demonstrated. The Brillouin interaction is responsible for the coupling between two optical waves and an acoustic wave when a resonance condition is fulfilled. Since the resonance condition is strain and temperaturedependent, by determining the resonance frequency we directly get a measure of temperature or strain. Local information about the acousto-optical resonance condition is typically obtained by using pulsed lightwaves and a classical time-of-flight technique (BOTDA technique). The main goal of this work has been the development of an innovative technique for the generation of optical signals, using a set of locked lasers – instead of the traditional techniques using external modulators. The utilisation of the injection-locking of semiconductor lasers is the key of the entire set-up and represents an entirely new and original approach, since it brings significant improvements in terms of SNR and costs. As long as intense pulses propagate along the fibre, the optical signals can be seriously degraded by several nonlinear interactions occurring inside the fibre; we show that the nonlinear effect exhibiting the lowest threshold power is the modulation instability (MI) process. From the study of the dynamic behaviour of MI we could observe the Fermi-Pasta-Ulam (FPU) recurrence over few periods in very comfortable conditions. One original application of Brillouin sensing has been the dosimetric measurement of ionising radiations in a nuclear environment. The measurement campaign has not only shown that distributed sensors based on Brillouin spectral analysis are radiation tolerant up to very high doses, but has also revealed the first observation – to our knowledge – of the negative compaction of silica in fibres. Distributed fibre sensors based on stimulated Brillouin scattering offer a unique capability for the analysis of optical signals and nonlinear phenomena in optical fibres. We present a generalised theoretical approach to the problem of localised sensing and report on the first distributed measurement – to our knowledge – of the parametric gain in a single-pump fibre-optics parametric amplifier (FOPA).

La diffusion Brillouin dans les fibres optiques

Among all non-linear optical effects observed in single-mode optical fibres, stimulated Brillouin scattering (SBS) is of particular importance since it has numerous practical implications. SBS occurs when laser waves are scattered through the interaction of light with hypersonic acoustic waves in the medium. It manifests through the generation of a backscattered Stokes wave that carries most of the input optical power once a definite intensity level is reached within the fibre core. It limits the maximum optical power that can be transmitted through an optical fibre and therefore can cause a severe penality for fibre optics telecommunications. The backscattered Stokes wave is down shifted in frequency with respect to the incident lightwave frequency. This frequency shift – often called the Brillouin frequency shift – depends on the fibre parameters and on the wavelength of the incident light. It is directly proportional to the acoustic velocity and ranges from 12 to 13 GHz for silica fibres at a 1.3 µm wavelength. The Brillouin frequency shift is also very sensitive to environmental quantities changing the acoustic velocity such as temperature and strain. This feature makes SBS very interesting for temperature and strain monitoring in optical fibres and has been used in the design of fibre optics sensors. In the present work, a novel method to measure SBS characteristics in single-mode optical fibres has been developed. It is based on the so-called pump and probe technique using two counterpropagating optical waves within the test fibre. It basically presents the originality to require only one laser source and relies on an electro-optic modulator to generate the probe signal by microwave modulation of the pump light. The inherent high stability of the experimental set-up has made possible the characterisation of different fibres in terms of SBS parameters with a higher accuracy than the traditional two lasers set-up. The influence of dopant concentration in silica fibres on the SBS properties has been fully characterised. Furthermore it has been determined that the presence of core dopants decreases the acoustic velocity resulting in a smaller Brillouin frequency shift. The temperature and strain effects on the SBS characteristics have been extensively investigated. The problem of the evolution of the polarisation of the interacting lightwaves has been studied and a model clarified the so far unexplained behaviour in low birefringence fibres. A new measurement procedure has been defined to achieve polarisation-independent Brillouin gain determination. The second facet of the present thesis deals with the concept of distributed fibre optics sensors based on SBS. The determination of the Brillouin frequency shift gives access to the temperature or strain experienced by the fibre, while a modified OTDR technique provides the information on the position. Here again the use of a single laser source together with an electro-optic modulator brings several advantages. Besides the convenient flexibility in the generation of the probe signal, it makes possible to pulse the optical signals to localise the interaction within the test fibre. The overall temperature or strain distribution of the test fibre can be carried out by measuring the Brillouin frequency shift at any locations throughout the test fibre. A sensor has been experimentally achieved and its performances can be summarised as follow: spatial resolution less than 10 meters over more than 10 kilometres, with a resolution on the Brillouin frequency determination of 1 MHz, that corresponds to a ±1°C temperature resolution or to a 2x10-5 strain resolution. The dynamic range can be increased up to 30 kilometres to the detriment of the spatial resolution. The ultimate performances of the SBS distributed fibre optics sensors have been investigated in terms of spatial resolution and dynamic range. It turns out that these sensors are eventually dedicated to distributed measurements over several tens of kilometres with a spatial resolution limited to the meter range. Finally two practical applications of such sensors are described: the measurement of the strain distribution in installed fibre optics cables for telecommunications and the temperature monitoring of electrical energy distribution cables. On site measurements using a Brillouin sensor have been performed for the first time thanks to the high stability and reliability of the sensor.

EPFL1997

Extreme temperature sensing using Brillouin scattering in optical fibers

Alexandre Fellay

Stimulated Brillouin scattering in silica-based optical fibers may be considered from two different and complementary standpoints. For a physicist, this interaction of light and pressure wave in a material, or equivalently in quantum theory terms between photons and phonons, gives some glimpses of the atomic structure of the solid and of its vibration modes. For an applied engineer, the same phenomenon may be put to good use as a sensing mechanism for distributed measurements, thanks to the dependence of the scattered light on external parameters such as the temperature, the pressure or the strain applied to the fiber. As far as temperature measurements are concerned, Brillouin-based distributed sensors have progressively gained wide recognition as efficient systems, even if their rather high cost still restricts the number of their applications. Yet they are generally used in a relatively narrow temperature range around the usual ambient temperature; in this domain, the frequency of the scattered light increases linearly with the increase in temperature. The extension of this range toward higher (up to 800°C) and lower (down to 1 K) temperature is the main aim of this thesis. In both cases, our measurements on various fiber samples show that the aforementioned linearity does not hold. Most notably, the characteristics of Brillouin scattering at low and very low temperature are strikingly different from those observed under normal conditions; they are directly related to the disordered nature of the silica that constitutes the fiber, what motivates the large place we here devote to the physics of amorphous solids. Despite the observed nonlinearities, our results demonstrate the feasibility of thermometry based on Brillouin scattering over the full investigated temperature range. We can thus swap in the last part of this work the physicist's point of view for that of an engineer and present the setup and the performances of a sensor, or rather of a whole family of sensors we have tested and improved in the course of the last few years; moreover, some real measurement examples are given. Finally, we propose some possibilities of further enhancement, that remain right now at the preliminary stage of their development.

EPFL2003

Gas traces measurement by photoacoustic spectroscopy using Helmholtz resonator-based sensors

Mario Mattiello

Photoacoustic spectroscopy is a well-established gas traces optical detection technique, which consists in the generation of an acoustic wave in the investigated gas compound excited by a modulated laser beam, and in the detection of this sound wave with a sensitive microphone. The sensitivity of this technique can be greatly enhanced through the use of acoustic resonators. A wide range of resonant configurations has been developed and reported in the literature in the last decades. Among these, Helmholtz resonators are known for their simplicity of implementation, though with a reduced efficiency. The main goal of this work is to demonstrate that Helmholtz resonators can be successfully applied to photoacoustic spectroscopy, delivering sensitivities in the same order of magnitude as other more common configurations, as well as offering a powerful tool to perform differential measurements. Two Helmholtz-based sensors are presented within this thesis. The first sensor has been developed for ammonia sensing, taking benefit from the properties of antimonide-based lasers; the final design has been the result of a carefully optimised compromise between high sensitivity, noise reduction, technical constraints, compact size and straightforward use. After several implemented improvements, an ultimate sub-ppm concentration detection limit has been achieved. The second sensor exploits the intrinsic phase shift existing between the two volumes of a Helmholtz resonator to perform differential measurements. Each of the two volumes of the resonator is filled with a different concentration of the same gas, whereas the exciting laser beam is split in two arms that separately illuminate the volumes, the resulting photoacoustic signal being proportional to the difference between the respective concentrations of the probed gas in the volumes. A particular detection scheme has been implemented to guarantee a linear measurement. The achieved sensitivity is not as high as obtained with the first sensor; nonetheless, the developed sensor offers the possibility to perform measurements that would otherwise require two different sensing devices, resulting in a clear gain in terms of cost and of detection complexity.

EPFL2008