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The Solar System is the gravitationally bound system of the Sun and the objects that orbit it. The largest of such objects are the eight planets, in order from the Sun: four terrestrial planets named Mercury, Venus, Earth and Mars, two gas giants named Jupiter and Saturn, and two ice giants named Uranus and Neptune. The terrestrial planets have a definite surface and are mostly made of rock and metal. The gas giants are mostly made of hydrogen and helium, while the ice giants are mostly made of 'volatile' substances such as water, ammonia, and methane. In some texts, these terrestrial and giant planets are called the inner Solar System and outer Solar System planets respectively. The Solar System was formed 4.6 billion years ago from the gravitational collapse of a giant interstellar molecular cloud. Over time, the cloud formed the Sun and a protoplanetary disk that gradually coalesced to form planets and other objects. That is the reason why all eight planets have an orbit that lies near the same plane. In the present day, 99.86% of the Solar System's mass is in the Sun and most of the remaining mass is contained in the planet Jupiter. Six planets, the six largest possible dwarf planets and many other bodies have natural satellites or moons orbiting around them. All giant planets and a few smaller bodies are encircled by planetary rings, composed of ice, dust and sometimes moonlets. There are an unknown number of smaller dwarf planets and innumerable small bodies orbiting the Sun. These objects are distributed in the asteroid belt that lies between the orbits of Mars and Jupiter, the Kuiper belt, the scattered disc that both lies beyond Neptune's orbit and at even further reaches of the Solar System which they would be classified as an extreme trans-Neptunian object. There is consensus among astronomers to these nine objects as dwarf planets: the asteroid , the Kuiper-belt objects Pluto, , , , and , and the scattered-disc objects , , and . Many small-body populations, including comets, centaurs and interplanetary dust clouds, freely travel between the regions of the Solar System.

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Structure determination techniques are an essential tool to investigate and understand molecules, especially in biology, where functionality crucially depends on structure. The dominant high-resolution methods, such as transmission electron microscopy and X-ray diffraction, rely on ensemble averaging, making them unsuitable for evidencing structural variations of flexible molecules. Common single-molecule imaging techniques like scanning probe microscopy achieve high resolution but lack access to 3D objects. A possible way to overcome these limitations is offered by low-energy electron holography (LEEH). So far, LEEH achieved molecular imaging at resolutions in the range of 7-8 Å on the single-molecule level. A resolution in the range of a few Å, which would give access to atomic details of molecular structures, is in theory attainable. Obtaining a resolution near the theoretical limit requires a fully optimized LEEH setup and workflow, for which in particular sample and emitter preparation are crucial. Here, I present a novel LEEH microscope with a unique experimental workflow, which is capable of resolving molecular substructures with an unprecedented resolution for LEEH experiments. The newly constructed LEEH microscope takes advantage of an efficient vibration isolation system and is remote-controlled to minimize external perturbations. The setup is capable of low-temperature (50 K) measurements, which enhances the stability of the system. A reliable way for preparing highly coherent electron emitters constituted by sharp tungsten tips is presented along with different methods for improving their performance via functionalization and UHV treatments. I show an optimized and reliable substrate preparation protocol resulting in ultra-clean free-standing single-layer graphene (SLG) samples. Native electrospray ion beam deposition (ES-IBD) allows for the transfer of non-volatile molecules from solution into gas phase and onto the substrate. By employing a quadrupole mass selection, highly pure molecular ion beams are obtained, which are soft-landed onto the SLG substrate in a controlled and reproducible manner while retaining an intact structure. This versatile preparation method allows us to study a great variety of molecules by LEEH. Data on proteins with masses ranging from 12-820 kDa reveal molecular shapes consistent with model structures. Locally, structural details as small as 5 Å were identified, thus we are approaching our goal of a resolution in the range of a few Å. The application of our methodology to flexible proteins, exemplified by antibodies, allowed for the imaging of their conformational variability and for determining the influence of the sample preparation on their structure. This gave us the possibility to directly image gas-phase related conformations. Data of compact molecular systems with masses below 3 kDa reveal that our LEEH microscope is able to investigate small molecules, such as porphyrines, at high imaging contrast. The presented results indicate that an optimized LEEH setup and workflow in combination with ES-IBD is a versatile microscopy method, which is filling the gap between high-resolution and single-molecule techniques by elucidating structural details of various molecular species.

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Ultra low quantum decoherence nano-optomechanical systems

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Thermal motion of a room-temperature mechanical resonator typically dominates the quantum backaction of its position measurement. This is a longstanding barrier for exploring cavity optomechanics at room temperature. In order to enter the quantum regime of the optomechanical interaction, we need to be in the "backaction-dominated" regime, where we can study the limits of quantum measurement and how to circumvent them. To create a system which can enter the quantum regime, the optomechanical transducer has to satisfy certain criteria. A quantum-enabled optomechanical system consists of an optical cavity and a mechanical resonator with ultra low quantum decoherence, which are strongly coupled to each other via the optomechanical interaction.High stress silicon nitride has enabled nanomechanical resonators with exceptionally low dissipation at room temperature via several soft-clamping techniques. Achieving high optomechanical coupling to these coherent nanobeams results in high optomechanical cooperativities, thus alleviating the thermal motion barrier for room temperature quantum optomechanics. Monolithic integration of high-Q nanobeam resonators with optical cavities has been limited to doubly-clamped nanobeams due to the complexity of the device fabrication and long device sizes required for conventional soft-clamping using phononic crystals. In addition, the previous demonstrations of such systems showed limited optomechanical couplings thus a limited single photon cooperativity.I present the design, fabrication and characterization of three different classes of nanomechanical resonators clamp-tapered, fractal-like, and polygon resonators, which support perimeter modes, with Q factors exceeding 3 billion at room temperature and their optical readout using an integrated nearfield nano-optomechanical transducer using high stress silicon nitride. Our transducer features a one-dimensional Fabry-Perot optical cavity integrated with a high-Q nanomechanical resonator. The Fabry-Perot optical cavity is formed by patterning two photonic crystal reflectors on a silicon nitride waveguide designed for high-Q optical modes. Our approach allows individual optimization of optical and mechanical resonators, while maintaining a high optomechanical coupling rate due to large optomechanical mode overlap. Our best performing devices show on-chip optomechanical transducers with single photon cooperativities as high as 123 with mechanical quality factor of 120 million at room temperature. The developed system is of great interest to the optomechanics and sensing community. In quantum optomechanics, it will serve as a platform for quantum feedback control of the nanomechanical resonators to achieve motional ground state of a macroscopic resonator and generation of squeezed light at room temperature. Owing to their record value mechanical quality factors, the room temperature force sensitivity of our highest Q perimeter modes is on par with atomic force microscopy cantilevers at millikelvin temperature.Complete documentation of a nanofabrication process is the key to its reproducibility. Process-specific details of the fabrication techniques are usually missing in journal publications. To bridge this gap, I developed NanoFab-net.org. An online open-access tool that allows sharing process-specific fabrication reports, extracting the metadata and obtaining a unique digital object identifier (DOI) for each report.

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Nanoscale modelling of ionic transport in the porous C-S-H network

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To reduce the CO2 footprint of construction materials, concrete producers blend their cement with Supplementary Cementitious Materials (SCMs). SCMs such as fly ash or blast furnace slag are mostly the byproducts of other industries. And while SCMs are chosen to match the properties of the common Ordinary Portland cement (OPC), their addition to the cement recipe may alter the chemistry of the system. These changes may lead to different mechanical and transport properties of the cement-based structure which may, in turn, affect its long-term resistance to harmful external agents. Therefore, understanding the relationship between cementâs microstructure and the degradation mechanisms is key for optimizing the design of new cementitious materialsIn this context, chloride attack is the most common reason for steel rebars to corrode especially when exposed to external chloride (seawater, deicer saltsâŠ). At low w/c ratios (typically 13) pore solution, the C-S-H surface develops a negative surface charge density. Electrostatic interactions between the surface and the ions in the pore solution result in a redistribution of the ionic species in two layers of charge at the interface of the solid i.e. the Electrical double layer (EDL). In nanoscopic pores, the EDL is dominated by atomic phenomena which are thought to interfere with the mobility of ions and chloride in particular. In order to understand and quantify the surface effects and their influence on ionic transport, we firstly propose an atomistic model of the EDL formation based on the use of the Metropolis Monte Carlo algorithm. This model is used to compute the ionic distributions and electrochemical potentials of electrolytes at equilibrium in nanoscopic pores. These quantities constitute the main driving forces of ionic transport at the pore scale. The microstructure parameters including the surface charge density of C-S-H, the ionic strength (and pH) of the pore solution, and the pore size are equally investigated and their effect on chlorideâs behavior quantified. Among the other parameters, the model also provides quantitative information on the effect of calcium ions which are thought to play a major role in the binding of chloride on C-S-H. The next step consists in using the calculated atomic-scale properties of the EDL in order to resolve the transport problem at the pore scale and compute microscopic diffusivities of chloride. This is achieved by using the molecular computations from the Monte Carlo (MC) engine in order to implement a modified version of the classical Poisson-Boltzmann system. The method is compared to the classical Finite element analysis of the Poisson-Nernst-Planck (PNP) equations and the data are discussed in the light of established experimental results in the literature.

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