Publication

Development of a MEMS Preconcentrator for Micro-gas Chromatography Analyses

Abstract

This paper presents the development of MEMS gas preconcentrator (GP) for the detection of trace level Volatile Organic Compounds (VOCs). Besides the development of the MEMS gas preconcentrator, we have also worked on the coupling of this preconcentration device with a micro gas chromatograph (μ-GC) for achieving an accurate detection system for gas trace monitoring. Preliminary results have highlighted a significant contribution of the MEMS GP on the μ-GC efficiency and a detection limit below 35ppbv for different vapors like toluene, vinyl acetate monomer, chloroform and methylisobutylketone was reported. © 2014 Published by Elsevier Ltd.

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Related concepts (15)
Gas chromatography–mass spectrometry
Gas chromatography–mass spectrometry (GC–MS) is an analytical method that combines the features of gas-chromatography and mass spectrometry to identify different substances within a test sample. Applications of GC–MS include drug detection, fire investigation, environmental analysis, explosives investigation, food and flavor analysis, and identification of unknown samples, including that of material samples obtained from planet Mars during probe missions as early as the 1970s.
Gas chromatography
Gas chromatography (GC) is a common type of chromatography used in analytical chemistry for separating and analyzing compounds that can be vaporized without decomposition. Typical uses of GC include testing the purity of a particular substance, or separating the different components of a mixture. In preparative chromatography, GC can be used to prepare pure compounds from a mixture. Gas chromatography is also sometimes known as vapor-phase chromatography (VPC), or gas–liquid partition chromatography (GLPC).
Electron ionization
Electron ionization (EI, formerly known as electron impact ionization and electron bombardment ionization) is an ionization method in which energetic electrons interact with solid or gas phase atoms or molecules to produce ions. EI was one of the first ionization techniques developed for mass spectrometry. However, this method is still a popular ionization technique. This technique is considered a hard (high fragmentation) ionization method, since it uses highly energetic electrons to produce ions.
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