Electron diffraction and high resolution transmission electron microscopy in the characterization of calcium phosphate precipitation from aqueous solutions under biomineralization conditions
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The microstructure of titanium alloys (Ti–1Al–1Mn, Ti–6Al–4V) nitrided under glow discharge was characterised using light microscopy, X-ray diffraction and analytical electron microscopy. The investigations revealed a complex multilayered microstructure pr ...
High-resolution transmission electron microscopy (HRTEM) and HRTEM simulation by the Bloch wave method (JEMS) are used to determine the structure and thickness of micro- and nanocrystals of biominerals and hydroxyapatite grown from aqueous solutions. It is ...
Information for phase identification may be gathered in the electron transmission microscope with spatial resolution down to the nanometre scale. Energy dispersive X-ray and electron energy loss spectrometries are based on inelastic electronsample interact ...
Zircaloy-4 has been oxidised in environmental scanning electron microscope (ESEM), at a temperature of 700 °C and the surface of the material has been observed during the oxidation, directly in the ESEM. The material has been subsequently analysed by atomi ...
Microstructure and chemical composition of the hard Ni–P–Ti layer formed on the Ti–6Al–4V alloy after duplex surface treatment were investigated by light microscopy, X-ray diffraction, scanning electron microscopy and analytical/high resolution transmissio ...
Information for phase identification may be gathered in the electron transmission microscope with spatial resolution down to the nanometre scale. Energy dispersive X-ray and electron energy loss spectrometries are based on inelastic electron/sample interac ...
The understanding of material self-assembling and self-organization mechanisms, at mesoscale, is crucial for nanotechnologies development. Such structures, hierarchically organized in superlattices or colloïdal crystals, are observed in inorganic or organo ...
A method for preparing and observing clay platelets for size and shape analysis using scanning electron microscopy (SEM) was developed. Samples of the clay platelets were prepared by polyelectrolyte-assisted adsorption onto a pyrolytic graphite surface. Th ...
Microorganisms were searched for among the complex microstructures observed on the surface of a fragment of the Tatahouine meteorite inherited from the Tunisian soil in which they were buried. In this view, the chemical compositions, particularly the nitro ...
Surface nitriding of tetragonal zirconia (t-ZrO2) has been performed with the aim of combining the optical properties of zirconium nitride (ZrN) with the hardness and toughening properties of tetragonal zirconia. A high current d.c. arc plasma source has b ...