Effect of recycled cellulose fibres on the properties of lightweight cement composite matrix

This paper discusses the results from an experimental investigation conducted to study the effect on using cellulose fibres as cement replacement on the properties of lightweight cement composite. The fibres were recycled from waste paper and packaging and the content in the composite was ranged from 0% to 16% by mass of cement. The prepared specimens were tested after 28 day of curing in order to investigate compressive and tensile strengths, density and thermal conductivity. Also, Scanning Electron Microscopy (SEM) examination was carried out.

Probing the local strength and toughness of microscopic hard second phases in metals and composites

Marco Cantoni, Raphaël Charvet, Cyril Dénéréaz, Willy Dufour, Marta Fornabaio, Lionel Michelet, Andreas Mortensen, Martin Guillermo Mueller, Václav Pejchal, Goran Zagar

Many engineering alloys and composites combine a ductile matrix with discrete microscopic reinforcing phases, e.g. silicon particles in aluminium alloys, carbides in steels or ceramic particles in metal matrix composites. It is well understood that the mechanical properties of such alloys and composites are strongly influenced by those of their reinforcing particles; yet not much is known of the nature and size of strength-limiting flaws within such microscopic second phases. To investigate the strength and fracture toughness of these microscopic particles directly, we have developed test methods that combine focused ion beam (FIB) milling with microtesting techniques and bespoke finite element simulation. Local strength is probed by micromachining individual reinforcing particles in such a way that tensile stresses are produced in a volume of material free of FIB and polishing artifacts upon the application of a load via nanoindenter. Fracture toughness is measured by the chevron-notch fracture test technique adapted for microscopic samples. Testing methods are established using nanocrystalline alumina fibers as the testbench material, so as to compare data thus obtained with known fiber properties from tensile tests on long sections of the fibers. These test methods are currently being transposed towards the microscopic testing of more irregularly shaped and anisotropic brittle second phases, with the objective to measure their local mechanical properties and identify microstructural flaws that govern the strength of such particles, using in-depth electron microscopy characterization combined with microtesting.

2015

Fracture toughness of weft-knitted fabric composites

Pierre-Etienne Bourban, Jan-Anders Månson, Ignaas Herman Johannes Verpoest

The mode I inter-laminar fracture toughness of advanced knitted textile composites was investigated. Two complex weft-knitted glass fabrics were selected for the study: a triple rib knit and a Milano knit were impregnated with a tough epoxy resin and tested using a double cantilever beam geometry. For both knitted composites, the influence of the growth direction was studied by investigating crack propagation in both the wale and course directions. The fracture toughness was quantified by determining the critical strain energy release rate (GIC) using the modified beam theory. The specimens had to be stiffened with layers of glass woven composites added on top and bottom of the beams. This was necessary in order to avoid plastic deformation of the beams and crack deviation out of the inter-laminar plane. The results clearly showed that knitted fabric composites have exceptional inter-laminar fracture toughness properties, namely, more than 7000 J/m2. The origin of the high GIC values, which are superior to woven or UD laminates, lies in the very complex fabric architecture. The threedimensional loop structure induces various energy consuming mechanisms, which do not occur in other composites. Toughening mechanisms such as crack branching, friction, yarn bridging and breakage were identified using scanning electron microscopy.

2002

Structural behavior and durability of multifunctional fiber-reinforced polymer components

Florian Riebel

In the context of sustainable development, building insulation represents a major concern as a means of increasing energy efficiency. In order to comply with new norms such as the Passive House standard, locations where load-bearing components must penetrate the building's insulating envelope, such as when cantilevered slabs (e.g. balconies) are anchored to building walls, constitute a particular challenge. With conventional steel reinforcement, thermal bridges are inevitable and insulation is weakened. To overcome this deficiency, a multifunctional joint has been developed in which GFRP (glass-fiber reinforced polymer) elements performthe necessary structural functions without compromising the continuity of the building's insulating envelope. This is due to GFRP materials' low thermal conductivity, which is magnitudes smaller than that of concrete and steel, making them particularly suitable. The anchorage of balconies requires linkages that can resist shear as well as tensile and compression forces in the upper and lower parts of the slab. In a first step, a hybrid joint was created in which the lower compression steel reinforcement was replaced by a compression-shear (CS-)element made of GFRP. This consisted of a short pultruded profile with cap plates bonded to its cut ends. In addition to compression forces, the element was intended to bear parts of the shear load. The joint was investigated in various full-scale beam specimens each representing a section of the slab. Based on the results, the joint's structural behavior was modeled analytically and structural requirements for the CS-element were determined. It was seen that shear transfer through the element increased with increasing shear-to-moment ratios. In a second step, an all-GFRP joint was created in which, in addition to the element in the compression zone, a tension-shear (TS-)element replaced the remaining steel reinforcement. This element consisted of the same pultruded profile cut to longer sections and penetrating the concrete. To anchor the tensile forces in the concrete, ribs were bonded to its surface. This joint type was also investigated through full-scale beam experiments similar to the hybrid-joint beams. The load transfer through the joint and into the concrete was studied and modeled analytically. The behavior of the all-GFRP joint was as ductile as that of the hybrid joints. The TS-element bore the main portion of the shear load independently of the shear-to-moment ratio however. The CS-element used in both joint types was of special interest with regard to remaining strength and stiffness after long-term service life. Exposure to alkaline concrete-pore solution represents a particular threat to the polyester matrix and glass fibers inside the GFRP material. Therefore, CS-elements were immersed in alkaline liquids at different temperatures and their compression strength and stiffness were studied during a period of eighteen months. Material degradation was investigated by SEM-microscopic images and EDX-analysis. The observed loss of compressive strength was ascribed to moisture diffusion and chemical degradation of the fibers, matrix, and fiber-matrix interface. It was shown that the strength degradation rate at different temperatures followed the Arrhenius rate law and that remaining strength after long time spans could therefore be projected by extrapolating the measurements. Remaining strength after 70 years of service life was found to be sufficient for the element never to become the critical failure location and classic concrete theory can be applied to verify the joint. Since stiffness at high temperatures was observed to already remain constant after short exposure times, this value could directly be extrapolated to apply to a 70-year service lifespan.

EPFL2006

Structural behavior and durability of multifunctional fiber-reinforced polymer components

Florian Riebel

EPFL2006