Analyse gravimétrique

Résumé

L’analyse gravimétrique décrit un ensemble de méthodes d'analyse chimique quantitative effectuée en déterminant par pesée, la masse d’un produit, l'analyte, formé ou éliminé. La variation de la masse peut avoir lieu par l’une des transformations suivantes : La variation de la masse peut être induite chimiquement (réaction chimique), thermiquement (analyse thermogravimétrique) ou électriquement (électrogravimétrie). Exemple d'une méthode d'analyse gravimétrique : l'analyse par combustion. Références Catégorie:Chimie analytique

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https://fr.wikipedia.org/wiki/Analyse_gravim%C3%A9trique

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La chimie analytique est la partie de la chimie qui concerne l'analyse des produits, c'est-à-dire l'identification et la caractérisation de substances chimiques connues ou non. La substance chimique

vignette|Formation d'un précipité d'hydroxyde de cobalt(II). En chimie et en métallurgie, un précipité est une phase dispersée hétérogène dans une phase majoritaire. La formation d'un précipité est la

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Next-generation DNA sequencing techniques

Wilhelm Ansorge

Next-generation high-throughput DNA sequencing techniques are opening fascinating opportunities in the life sciences. Novel fields and applications in biology and medicine are becoming a reality, beyond the genomic sequencing which was original development goal and application. Serving as examples are: personal genomics with detailed analysis of individual genome stretches; precise analysis of RNA transcripts for gene expression, surpassing and replacing in several respects analysis by various microarray platforms, for instance in reliable and precise quantification of transcripts and as a tool for identification and analysis of DNA regions interacting with regulatory proteins in functional regulation of gene expression. The next-generation sequencing technologies offer novel and rapid ways for genome-wide characterisation and profiling of mRNAs, small RNAs, transcription factor regions, structure of chromatin and DNA methylation patterns, microbiology and metagenomics. In this article, development of commercial sequencing devices is reviewed and some European contributions to the field are mentioned. Presently commercially available very high-throughput DNA sequencing platforms, as well as techniques under development, are described and their applications in bio-medical fields discussed.

2009

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Spectroscopy of 3, 4, 9, 10-perylenetetracarboxylic dianhydride (PTCDA) attached to rare gas samples: Clusters vs. bulk matrices. I. Absorption spectroscopy

Matthieu Dvorak, Wolfgang Harbich, Stefan Minniberger, Alexandre Rydlo

The interaction between 3, 4, 9, 10-perylenetetracarboxylic dianhydride (PTCDA) and rare gas or para-hydrogen samples is studied by means of laser-induced fluorescence excitation spectroscopy. The comparison between spectra of PTCDA embedded in a neon matrix and spectra attached to large neon clusters shows that these large organic molecules reside on the surface of the clusters when doped by the pick-up technique. PTCDA molecules can adopt different conformations when attached to argon, neon, and para-hydrogen clusters which implies that the surface of such clusters has a well-defined structure without liquid or fluxional properties. Moreover, a precise analysis of the doping process of these clusters reveals that the mobility of large molecules on the cluster surface is quenched, preventing agglomeration and complex formation. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.4759443]

American Institute of Physics2012

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The role of malachite nanorods for the electrochemical reduction of CO2 to C-2 hydrocarbons

Emadeddin Oveisi, Mariana Spodaryk, Jie Zhang, Kun Zhao

The electrochemical reduction of CO2 to higher hydrocarbons is a very challenging process that has high potential for the storage of large amounts of renewable energy with a high gravimetric and volumetric energy density. The distribution of hydrocarbons from the electrocatalytic reduction of CO2 is primarily determined by the interaction of the cathode material with the CO2 in the electrolyte. While the research on the electrochemical CO2 reduction focuses on the cathode metal and surface structure of the metals, recently evidence was found that the metal itself may not be the active species but rather the product formed from the metal and CO2. In this paper, we report about the synthesis, catalytic activity and selectivity of nanostructured metal carbonate, i.e. malachite, as a highly active catalyst for the electrochemical synthesis of C2 hydrocarbons. These first results obtained on Cu-2(OH)(2)CO3 nanorod-structured "trees" show that carbonate, not the pure metal, is the active catalytic species. This new catalyst favors the production of ethylene (C2H4) and ethane (C2H6) with significantly higher Faradaic efficiency than that of the pure Cu surface. (C) 2018 Elsevier Ltd. All rights reserved.

PERGAMON-ELSEVIER SCIENCE LTD2019

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